Technology Process of Benzene, 1-ethyl-4-(2-methoxy-1-methylethyl)-
There total 6 articles about Benzene, 1-ethyl-4-(2-methoxy-1-methylethyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; tetra-(n-butyl)ammonium iodide;
1.) petroleum ether, 30 min; 2.) 4 h;
DOI:10.1016/S0040-4020(01)87425-1
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 89 percent / sodium borohydride, 2 M NaOH / ethanol; H2O / Ambient temperature
2: 73 percent / conc. sulphuric acid / toluene / 24 h / Heating
3: 68 percent / aluminium chloride / CH2Cl2 / 22 h / Ambient temperature
4: 63 percent / 20percent aq. Na2CO3 / 3 h / Ambient temperature
5: 81 percent / hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
6: 32 percent / 1.) tetrabutylammonium iodide, 12 M NaOH / 1.) petroleum ether, 30 min; 2.) 4 h
With
potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; aluminium trichloride; sulfuric acid; tetra-(n-butyl)ammonium iodide; sodium carbonate; hydrazine hydrate;
In
ethanol; dichloromethane; water; toluene; diethylene glycol;
DOI:10.1016/S0040-4020(01)87425-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 73 percent / conc. sulphuric acid / toluene / 24 h / Heating
2: 68 percent / aluminium chloride / CH2Cl2 / 22 h / Ambient temperature
3: 63 percent / 20percent aq. Na2CO3 / 3 h / Ambient temperature
4: 81 percent / hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 1 h / Heating
5: 32 percent / 1.) tetrabutylammonium iodide, 12 M NaOH / 1.) petroleum ether, 30 min; 2.) 4 h
With
potassium hydroxide; sodium hydroxide; aluminium trichloride; sulfuric acid; tetra-(n-butyl)ammonium iodide; sodium carbonate; hydrazine hydrate;
In
dichloromethane; toluene; diethylene glycol;
DOI:10.1016/S0040-4020(01)87425-1