1-Butanesulfonic acid, 4-(phenylamino)-

Base Information

Chemical Name:1-Butanesulfonic acid, 4-(phenylamino)-
CAS No.:94624-92-7
Molecular Formula:C10H15NO3S
Molecular Weight:229.3
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Butanesulfonic acid, 4-(phenylamino)-

Chemical Property:

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Technology Process of 1-Butanesulfonic acid, 4-(phenylamino)-

There total 1 articles about 1-Butanesulfonic acid, 4-(phenylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1633-83-6
1,4-butane sultone

: 62-53-3
aniline

: 94624-92-7
4-anilino-1-butanesulfonic acid

Guidance literature:

Reference yield:

: 94624-92-7
4-anilino-1-butanesulfonic acid

: 4-Anilino-butanesulfonic acid sodium salt

Guidance literature:: With aniline; In ethanol; water;

Reference yield:

: 94624-92-7
4-anilino-1-butanesulfonic acid

: 905975-36-2
[1-benzyl-2-(1,1-dioxo-2-phenyl-1λ⁶-[1,2]thiazinan-6-ylidene)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: POCl₃ / Heating

2.1: K₂CO₃ / ethyl acetate / 20 °C

3.1: n-BuLi / hexane; tetrahydrofuran / 20 °C

3.2: 48 percent / tetrahydrofuran; hexane / -78 °C

4.1: n-BuLi / hexane; tetrahydrofuran / -78 - 20 °C

4.2: 65 percent / tetrahydrofuran; hexane

With n-butyllithium; potassium carbonate; trichlorophosphate; In tetrahydrofuran; hexane; ethyl acetate; 3.2: Wittig-Horner reaction / 4.2: Wittig-Horner reaction;
DOI:10.1016/j.bmcl.2006.04.079