Technology Process of Benzoic acid,
2-heptyl-4-[3-heptyl-5-hydroxy-2-(methoxycarbonyl)phenoxy]-3,6-dimeth
oxy-, methyl ester
There total 4 articles about Benzoic acid,
2-heptyl-4-[3-heptyl-5-hydroxy-2-(methoxycarbonyl)phenoxy]-3,6-dimeth
oxy-, methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / K2CO3 / acetone / 3 h / Heating
2: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 6 h
3: 78 percent / K2CO3 / 2-methyl-propan-2-ol / 16 h / Heating
4: 1.) Br2, AcOH, 2.) HBr / 1.) CCl4, Ac2O, a) RT, 0.5 h, b) reflux, 3 h 2.) CCl4, AcOH, H2O, reflux, 2 h
With
hydrogen bromide; hydrogen; bromine; potassium carbonate; acetic acid;
palladium on activated charcoal;
In
ethyl acetate; acetone; tert-butyl alcohol;
DOI:10.1071/CH9842349
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 6 h
2: 78 percent / K2CO3 / 2-methyl-propan-2-ol / 16 h / Heating
3: 1.) Br2, AcOH, 2.) HBr / 1.) CCl4, Ac2O, a) RT, 0.5 h, b) reflux, 3 h 2.) CCl4, AcOH, H2O, reflux, 2 h
With
hydrogen bromide; hydrogen; bromine; potassium carbonate; acetic acid;
palladium on activated charcoal;
In
ethyl acetate; tert-butyl alcohol;
DOI:10.1071/CH9842349
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / K2CO3 / 2-methyl-propan-2-ol / 16 h / Heating
2: 1.) Br2, AcOH, 2.) HBr / 1.) CCl4, Ac2O, a) RT, 0.5 h, b) reflux, 3 h 2.) CCl4, AcOH, H2O, reflux, 2 h
With
hydrogen bromide; bromine; potassium carbonate; acetic acid;
In
tert-butyl alcohol;
DOI:10.1071/CH9842349
