methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Base Information

Chemical Name:methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate
CAS No.:94693-40-0
Molecular Formula:C₃₃H₄₈O₈
Molecular Weight:572.739
Hs Code.:

Synonyms:methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Suppliers and Price of methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

There total 5 articles about methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 94693-39-7
methyl 2-heptyl-4-(3-heptyl-5-hydroxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

: 74-88-4
methyl iodide

: 94693-40-0
methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl acetamide; for 3h; Ambient temperature;
DOI:10.1071/CH9842349

Reference yield:

: 60139-12-0
methyl 4-benzyloxy-2-heptyl-3-hydroxy-6-methoxybenzoate

: 94693-40-0
methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / K₂CO₃ / acetone / 3 h / Heating

2: 90 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h

3: 78 percent / K₂CO₃ / 2-methyl-propan-2-ol / 16 h / Heating

4: 1.) Br₂, AcOH, 2.) HBr / 1.) CCl₄, Ac₂O, a) RT, 0.5 h, b) reflux, 3 h 2.) CCl₄, AcOH, H₂O, reflux, 2 h

5: 94 percent / K₂CO₃ / N,N-dimethyl-acetamide / 3 h / Ambient temperature

With hydrogen bromide; hydrogen; bromine; potassium carbonate; acetic acid; palladium on activated charcoal; In N,N-dimethyl acetamide; ethyl acetate; acetone; tert-butyl alcohol;
DOI:10.1071/CH9842349

Reference yield:

: 94693-32-0
methyl 4-benzyloxy-2-heptyl-3,6-dimethoxybenzoate

: 94693-40-0
methyl 2-heptyl-4-(3-heptyl-5-methoxy-2-methoxycarbonylphenoxy)-3,6-dimethoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h

2: 78 percent / K₂CO₃ / 2-methyl-propan-2-ol / 16 h / Heating

3: 1.) Br₂, AcOH, 2.) HBr / 1.) CCl₄, Ac₂O, a) RT, 0.5 h, b) reflux, 3 h 2.) CCl₄, AcOH, H₂O, reflux, 2 h

4: 94 percent / K₂CO₃ / N,N-dimethyl-acetamide / 3 h / Ambient temperature

With hydrogen bromide; hydrogen; bromine; potassium carbonate; acetic acid; palladium on activated charcoal; In N,N-dimethyl acetamide; ethyl acetate; tert-butyl alcohol;
DOI:10.1071/CH9842349