Mercury, chloro(5-phenoxy-1-pentenyl)-, (E)-

Base Information

Chemical Name:Mercury, chloro(5-phenoxy-1-pentenyl)-, (E)-
CAS No.:94807-42-8
Molecular Formula:C11H13ClHgO
Molecular Weight:397.267
Hs Code.:

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Chemical Property of Mercury, chloro(5-phenoxy-1-pentenyl)-, (E)-

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Technology Process of Mercury, chloro(5-phenoxy-1-pentenyl)-, (E)-

There total 1 articles about Mercury, chloro(5-phenoxy-1-pentenyl)-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 92635-84-2
(E)-5-phenoxy-1-pentenylboronic acid

: 1600-27-7
mercury(II) diacetate

: 94807-42-8
(E)-5-phenoxy-1-pentenylmercuric chloride

Guidance literature:: With sodium chloride; In tetrahydrofuran; addn. of mercury acetate in small portions to boronic acid soln., room temp.; stirring, 15 min; addn. to aq. NaCl soln.; immediate pptn.; stirring, 30 min; filtration: washing (water); dissoln. in chloroform; drying(MgSO4); concentrating; pptn.; recrystn. (diethyl ether);
DOI:10.1016/0022-328X(84)80477-5

Reference yield: 95.0%

: 94807-42-8
(E)-5-phenoxy-1-pentenylmercuric chloride

: 94807-43-9
di-1-[(E)-5-phenoxy-1-pentenyl]mercury

Guidance literature:: With Na₂SnO₂; In tetrahydrofuran; addn. of alkaline sodium stannite to the well stirred vinylmercuric chloride soln., room temp.; stirring, 0°C, 2h; keeping at 10°C overnight; extn. (diethyl ether); washing organic layers with water; drying (MgSO4); evapn.; chromy. (silica gel, petroleum ether/ether 90/10); recrystn. (diethyl ether); elem. anal.;
DOI:10.1016/0022-328X(84)80477-5