1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone]

Base Information

Chemical Name:1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone]
CAS No.:94829-99-9
Molecular Formula:C19H18N4O5
Molecular Weight:382.376
Hs Code.:
DSSTox Substance ID:DTXSID701127131

Synonyms:DTXSID701127131;1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone];94829-99-9

Suppliers and Price of 1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone]

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:382.12771969
Heavy Atom Count:28
Complexity:596

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)[N+](=O)[O-])NN=CCCCN2C(=O)C3=CC=CC=C3C2=O

Technology Process of 1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone]

There total 4 articles about 1,3-Dihydro-1,3-dioxo-2H-isoindole-2-butanal 2-[2-(2-methoxy-5-nitrophenyl)hydrazone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 94829-98-8
(2-methoxy-5-nitrophenyl)hydrazine

: 94829-99-9
2-methoxy-5-nitrophenylhydrazone of γ-phtalimidobutyraldehyde

Guidance literature:: With phosphoric acid; In ethanol; benzene; 1.) 3 h, reflux, 2.) 48 h, 20 deg C_.;
DOI:10.1007/BF00506393

Reference yield:

: 25543-10-6
N-methoxycarbonylphthalimide

: 94829-99-9
2-methoxy-5-nitrophenylhydrazone of γ-phtalimidobutyraldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / ethanol / 2 h / Heating

2: 85percent phosphoric acid / ethanol; benzene / 1.) 3 h, reflux, 2.) 48 h, 20 deg C_.

With phosphoric acid; In ethanol; benzene;
DOI:10.1007/BF00506393

Reference yield:

: 1074-82-4
potassium phtalimide

: 94829-99-9
2-methoxy-5-nitrophenylhydrazone of γ-phtalimidobutyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / dimethylformamide / 1.) 1 h, 20 deg C, 2.) 2 h, 70-75 deg C_.

2: 93 percent / ethanol / 2 h / Heating

3: 85percent phosphoric acid / ethanol; benzene / 1.) 3 h, reflux, 2.) 48 h, 20 deg C_.

With phosphoric acid; In ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1007/BF00506393