1,3-Dithiane, 2,2-bis(4-methylphenyl)-

Base Information

Chemical Name:1,3-Dithiane, 2,2-bis(4-methylphenyl)-
CAS No.:94996-75-5
Molecular Formula:C18H20S2
Molecular Weight:300.489
Hs Code.:
DSSTox Substance ID:DTXSID30446593
Nikkaji Number:J633.266H
Wikidata:Q82265302

Synonyms:1,3-Dithiane, 2,2-bis(4-methylphenyl)-;2,2-bis(4-methylphenyl)-1,3-dithiane;94996-75-5;DTXSID30446593;10.14272/HXQGJLZXQGNWMG-UHFFFAOYSA-N;doi:10.14272/HXQGJLZXQGNWMG-UHFFFAOYSA-N

Suppliers and Price of 1,3-Dithiane, 2,2-bis(4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dithiane, 2,2-bis(4-methylphenyl)-

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:300.10064299
Heavy Atom Count:20
Complexity:269

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C2(SCCCS2)C3=CC=C(C=C3)C

Technology Process of 1,3-Dithiane, 2,2-bis(4-methylphenyl)-

There total 4 articles about 1,3-Dithiane, 2,2-bis(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 109-80-8
1.3-propanedithiol

: 611-97-2
bis(p-methylphenyl)-methanone

: 94996-75-5
2,2-di-(p-methylphenyl)-1,3-dithiane

Guidance literature:: With silica gel; iron(III) chloride; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81203-5

Reference yield:

: 611-97-2
bis(p-methylphenyl)-methanone

: 94996-75-5
2,2-di-(p-methylphenyl)-1,3-dithiane

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / BF₃*Et₂O / benzene / 24 h / Ambient temperature

2: 96 percent / 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate, oxygen / CH₂Cl₂ / 0.3 h / Irradiation

3: 92 percent / FeCl₃-silica gel / CH₂Cl₂ / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; oxygen; silica gel; iron(III) chloride; 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate; In dichloromethane; benzene;
DOI:10.1016/S0040-4020(01)81203-5

Reference yield:

: 144918-41-2
C₂₇H₂₄S₂

: 94996-75-5
2,2-di-(p-methylphenyl)-1,3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate, oxygen / CH₂Cl₂ / 0.3 h / Irradiation

2: 92 percent / FeCl₃-silica gel / CH₂Cl₂ / 3 h / Ambient temperature

With oxygen; silica gel; iron(III) chloride; 2,4,6-tris(p-chlorophenyl)pyrylium perchlorate; In dichloromethane;
DOI:10.1016/S0040-4020(01)81203-5