3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl-

Base Information

• Chemical Name: 3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl-
• CAS No.: 127040-36-2
• Molecular Formula: C₁₇H₁₆N₂O
• Molecular Weight: 264.327
• DSSTox Substance ID: DTXSID30155370
• Wikidata: Q83023269
• Mol file: 127040-36-2.mol

Synonyms:BRN 4259143;3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl-;127040-36-2;11H-3-Oxo-6,6-dimethyl-3,4,5,6-tetrahydropyrido(3,2-a)carbazole;4,5,6,11-Tetrahydro-6,6-dimethyl-3H-pyrido(3,2-a)carbazol-3-one;DTXSID30155370;LS-133331

Chemical Property of 3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl-

Chemical Property:

• Vapor Pressure: 4.48E-13mmHg at 25°C
• Boiling Point: 571.6°Cat760mmHg
• Flash Point: 299.5°C
• Density: 1.29g/cm³
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 264.126263138
• Heavy Atom Count: 20
• Complexity: 517

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1(CC2=C(C=CC(=O)N2)C3=C1C4=CC=CC=C4N3)C

Technology Process of 3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl-

There total 1 articles about 3H-Pyrido(3,2-a)carbazol-3-one, 4,5,6,11-tetrahydro-6,6-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

7,7-Dimethyl-7,8-dihydro-2,5-(1H,6H)-quinolinedione (55119-00-1) + phenylhydrazine hydrochloride (59-88-1) → 11H-3-oxo-6,6-dimethyl-3,4,5,6-tetrahydropyrido<3,2-a>carbazole (127040-36-2)

Guidance literature:

In acetic acid; for 5h; Heating;

DOI:10.1007/BF00764806

upstream raw materials:

7,7-Dimethyl-7,8-dihydro-2,5-(1H,6H)-quinolinedione

phenylhydrazine hydrochloride