N2-(4-Fluorophenyl)-N1,N1-dimethylmethanimidamide

Base Information

• Chemical Name: N2-(4-Fluorophenyl)-N1,N1-dimethylmethanimidamide
• CAS No.: 15851-81-7
• Molecular Formula: C9H11 F N2
• Molecular Weight: 166.198
• Hs Code.: 2925290090
• Mol file: 15851-81-7.mol

Synonyms:Formamidine,N'-(p-fluorophenyl)-N,N-dimethyl- (8CI); NSC 101579

Chemical Property of N2-(4-Fluorophenyl)-N1,N1-dimethylmethanimidamide

Chemical Property:

• Boiling Point: 227.7oC at 760 mmHg
• Flash Point: 91.5oC
• PSA: 15.60000
• Density: 1g/cm3
• LogP: 2.04710

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N2-(4-Fluorophenyl)-N1,N1-dimethylmethanimidamide

There total 4 articles about N2-(4-Fluorophenyl)-N1,N1-dimethylmethanimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N-dimethyl-formamide dimethyl acetal (4637-24-5) + 4-fluoroaniline (371-40-4) → N.N-Dimethyl-N'-(4-fluorophenyl)formamidin (15851-81-7)

Guidance literature:

In neat (no solvent); at 80 ℃; Microwave irradiation;

DOI:10.1016/j.tet.2020.131205

Reference yield: 42.0%

→ N.N-Dimethyl-N'-(4-fluorophenyl)formamidin (15851-81-7)

Guidance literature:

Reference yield:

para-fluorophenyl isocyanate (1195-45-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N.N-Dimethyl-N'-(4-fluorophenyl)formamidin (15851-81-7)

Guidance literature:

DOI:10.1021/jo00887a017

upstream raw materials:

N,N-dimethyl-formamide

4-fluoroaniline

para-fluorophenyl isocyanate

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

ethyl 1-(4-fluorophenyl)-1H-imidazole-4-carboxylate

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