Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-

Base Information

Chemical Name:Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-
CAS No.:747-80-8
Molecular Formula:C21H24B3N3
Molecular Weight:350.875
Hs Code.:
NSC Number:157566
DSSTox Substance ID:DTXSID90303259
Wikidata:Q82048443

Synonyms:Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-;747-80-8;NSC157566;SCHEMBL1158297;DTXSID90303259;NSC-157566;Borazine,4,6-trimethyl-1,3,5-triphenyl-

Suppliers and Price of Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-

Chemical Property:

Vapor Pressure:1.76E-07mmHg at 25°C
Boiling Point:426.5°Cat760mmHg
Flash Point:211.7°C
Density:1.07g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:351.2249383
Heavy Atom Count:27
Complexity:377

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(N(B(N(B(N1C2=CC=CC=C2)C)C3=CC=CC=C3)C)C4=CC=CC=C4)C

Technology Process of Borazine, 2,4,6-trimethyl-1,3,5-triphenyl-

There total 13 articles about Borazine, 2,4,6-trimethyl-1,3,5-triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 917-64-6
methyl magnesium iodide

: 981-87-3
B-trichloro-N-triphenylborazine

: 747-80-8
2,4,6-trimethyl-1,3,5-triphenyl-borazine

Guidance literature:: In diethyl ether; under dry nitrogen, addn. of a suspn. of CH3MgI to a soln. of B-compound, refluxing for 1 h; cooling, addn. of an aq. soln. of NH4Cl, filtn., washing (Et2O), drying organic layers (CaCl2), evapn. to dryness under reduced pressure;
DOI:10.1016/0022-328X(94)80079-0

Reference yield: 11.0%

: 142-04-1,36663-09-9
aniline hydrochloride

: N,N-dimethyl-aniline; compound with boron chloride

: 747-80-8
2,4,6-trimethyl-1,3,5-triphenyl-borazine

Guidance literature:: With methyl magnesium iodide; ammonium chloride; In chlorobenzene; (dry Ar); refluxed 6 h, CH3MgI added dropwise, refluxed 1 h, cooled (ice bath), quenched with a aq. soln. of NH4Cl; pptd. by addition of methanol to a Et2O-soln.;
DOI:10.1016/S0020-1693(00)85349-9

Reference yield:

: 17933-16-3
dibromomethylborane

: 17729-33-8
N,N-bis(trimethylstannyl)phenylamine

: 5158-50-9
dimethylboron bromide

: 747-80-8
2,4,6-trimethyl-1,3,5-triphenyl-borazine

: 1066-44-0
trimethyltin bromide

: bis(bromomethylboryl)phenylamine

Guidance literature:: In dichloromethane; N2 atmosphere, addn. of soln. of stannyl compound to soln. of borane at -65 to -75°C (30 min), slow warming to room temp., stirring (roomtemp., 16 h); (5)B-NMR-monitoring, PhN(BBrMe)2/Me2BBr/(PhNBMe)3 ratio 12.5:1.5:0.6, not isolated;