Technology Process of 9(10H)-Acridinone, 10-(4-chlorophenyl)-
There total 5 articles about 9(10H)-Acridinone, 10-(4-chlorophenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide;
In
dimethyl sulfoxide;
at 120 ℃;
for 48h;
under 760.051 Torr;
DOI:10.1039/c2cc35425j
- Guidance literature:
-
With
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate;
In
toluene;
at 100 ℃;
for 24h;
Inert atmosphere;
Sealed tube;
DOI:10.1055/s-0037-1612256
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bis-triphenylphosphine-palladium(II) chloride; potassium phosphate / toluene / 8 h / 100 °C / Inert atmosphere; Sealed tube
2: tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; 1,1'-bis-(diphenylphosphino)ferrocene / toluene / 24 h / 100 °C / Inert atmosphere; Sealed tube
With
bis-triphenylphosphine-palladium(II) chloride; 1,1'-bis-(diphenylphosphino)ferrocene; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate;
In
toluene;
1: |Suzuki-Miyaura Coupling / 2: |Buchwald-Hartwig Coupling;
DOI:10.1055/s-0037-1612256