Cyclobutanone, 2-[bis(phenylmethyl)amino]-

Base Information

• Chemical Name: Cyclobutanone, 2-[bis(phenylmethyl)amino]-
• CAS No.: 95588-06-0
• Molecular Formula: C18H19NO
• Molecular Weight: 265.355

Synonyms:2-(Dibenzylamino)cyclobutanon;2-dibenzylaminocyclobutanone;2-(dibenzylamino)cyclobutanone;α-dibenzylamino cyclobutanone;2-Dibenzylamino-cyclobutanone;

Chemical Property of Cyclobutanone, 2-[bis(phenylmethyl)amino]-

Chemical Property:

• PSA: 20.31000
• LogP: 3.42030

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclobutanone, 2-[bis(phenylmethyl)amino]-

There total 3 articles about Cyclobutanone, 2-[bis(phenylmethyl)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-hydroxycyclobutanone (99440-99-0) + dibenzylamine (103-49-1) → α-dibenzylaminocyclobutanone (95588-06-0)

Guidance literature:

With dmap; In toluene; at 20 ℃; for 15h;

DOI:10.1016/j.tet.2016.10.024

Reference yield: 60.79%

1,2-bis(trimethylsiloxy)cyclobutene (17082-61-0) + dibenzylamine (103-49-1) → α-dibenzylaminocyclobutanone (95588-06-0)

Guidance literature:

In methanol; at 0 - 20 ℃;

Reference yield: 38.93%

2-hydroxycyclobutanone (99440-99-0) + diphenylamine (122-39-4) → α-dibenzylaminocyclobutanone (95588-06-0)

Guidance literature:

In 1,4-dioxane; at 20 ℃; for 16h;

upstream raw materials:

1,2-bis(trimethylsiloxy)cyclobutene

dibenzylamine

2-hydroxycyclobutanone

diphenylamine

Downstream raw materials:

(1R,2R)- and (1S,2S)-1-Hydroxy-2-cyclobutane-1-acetic acid, t-butyl ester

(1R,2S)- and (1S,2R)-1-hydroxy-2-cyclobutane-1-acetic acid, t-butyl ester

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