6-methyl-2-pyridinecarboxaldehyde semicarbazone

Base Information

• Chemical Name: 6-methyl-2-pyridinecarboxaldehyde semicarbazone
• CAS No.: 90953-04-1
• Molecular Formula: C₈H₁₀N₄O
• Molecular Weight: 178.194
• Mol file: 90953-04-1.mol

Synonyms:Picolinaldehyde,6-methyl-, semicarbazone (6CI,7CI)

Chemical Property of 6-methyl-2-pyridinecarboxaldehyde semicarbazone

Chemical Property:

• PSA: 81.36000
• LogP: 1.29690

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-methyl-2-pyridinecarboxaldehyde semicarbazone

There total 4 articles about 6-methyl-2-pyridinecarboxaldehyde semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-lutidine N-oxide (1073-23-0) → 6-Methyl-pyridin-aldehyd-(2)-semicarbazon (90953-04-1)

Guidance literature:

Multi-step reaction with 4 steps

2: hydrogenchloride

3: manganese(IV) oxide; diethyl ether

With hydrogenchloride; manganese(IV) oxide; diethyl ether;

Reference yield:

2-(Hydroxymethyl)-6-methylpyridine (1122-71-0) → 6-Methyl-pyridin-aldehyd-(2)-semicarbazon (90953-04-1)

Guidance literature:

Multi-step reaction with 2 steps

1: manganese(IV) oxide; diethyl ether

With manganese(IV) oxide; diethyl ether;

Reference yield:

acetic acid 6-methyl-pyridin-2-ylmethyl ester (13287-64-4) → 6-Methyl-pyridin-aldehyd-(2)-semicarbazon (90953-04-1)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogenchloride

2: manganese(IV) oxide; diethyl ether

With hydrogenchloride; manganese(IV) oxide; diethyl ether;

upstream raw materials:

6-methyl-2-pyridinecarboxaldehyde

2,6-lutidine N-oxide

2-(Hydroxymethyl)-6-methylpyridine

acetic acid 6-methyl-pyridin-2-ylmethyl ester