Cyclohexanecarboxylic acid, 4-acetyl-2-[(1,4,5-trimethoxy-2-naphthalenyl)methyl]-, methyl ester

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 4-acetyl-2-[(1,4,5-trimethoxy-2-naphthalenyl)methyl]-, methyl ester
CAS No.:95636-38-7
Molecular Formula:C24H30O6
Molecular Weight:414.499
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanecarboxylic acid, 4-acetyl-2-[(1,4,5-trimethoxy-2-naphthalenyl)methyl]-, methyl ester

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Technology Process of Cyclohexanecarboxylic acid, 4-acetyl-2-[(1,4,5-trimethoxy-2-naphthalenyl)methyl]-, methyl ester

There total 21 articles about Cyclohexanecarboxylic acid, 4-acetyl-2-[(1,4,5-trimethoxy-2-naphthalenyl)methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4893-15-6
1-(4-methoxy-cyclohex-3-enyl)-ethanone

: 95636-38-7
methyl-2-(1,4,5-trimethoxynaphth-2-yl)methyl-4-acetylcyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 13 steps

1: NaBH₄

2: hydrolysis

4: NaH

6: 81 percent / LDA

7: 90 percent

8: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

9: K₂CO₃

10: BF₃, EtSH

11: CrO₃, acid

12: 2.) air / 1.) benzene, 45 deg C, 24 h.

13: K₂CO₃ / acetone

With chromium(VI) oxide; sodium hydroxide; sodium tetrahydroborate; air; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide; In acetone;
DOI:10.1021/ja00215a058

Reference yield:

: 113507-59-8
4-(hydroxyethyl)cyclohexanone

: 95636-38-7
methyl-2-(1,4,5-trimethoxynaphth-2-yl)methyl-4-acetylcyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 11 steps

2: NaH

4: 81 percent / LDA

5: 90 percent

6: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

7: K₂CO₃

8: BF₃, EtSH

9: CrO₃, acid

10: 2.) air / 1.) benzene, 45 deg C, 24 h.

11: K₂CO₃ / acetone

With chromium(VI) oxide; sodium hydroxide; air; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide; In acetone;
DOI:10.1021/ja00215a058

Reference yield:

: 113507-58-7
1-(4-Methoxy-cyclohex-3-enyl)-ethanol

: 95636-38-7
methyl-2-(1,4,5-trimethoxynaphth-2-yl)methyl-4-acetylcyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 12 steps

1: hydrolysis

3: NaH

5: 81 percent / LDA

6: 90 percent

7: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

8: K₂CO₃

9: BF₃, EtSH

10: CrO₃, acid

11: 2.) air / 1.) benzene, 45 deg C, 24 h.

12: K₂CO₃ / acetone

With chromium(VI) oxide; sodium hydroxide; air; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide; In acetone;
DOI:10.1021/ja00215a058