9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]-

Base Information

Chemical Name:9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]-
CAS No.:95636-48-9
Molecular Formula:C26H22O6S
Molecular Weight:462.523
Hs Code.:

Synonyms:

Suppliers and Price of 9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]-

There total 15 articles about 9,10-Anthracenedione, 1-hydroxy-8-methoxy-2-[1-oxo-2-(phenylsulfinyl)pentyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 92811-05-7
1-hydroxy-8-methoxy-2-(1'-oxo-2'-phenylthiopentyl)anthraquinone

: 95636-48-9
1-hydroxy-8-methoxy-2-(1-oxo-2-sulfoxophenylpentyl)anthraquinone

Guidance literature:: With sodium periodate; In water; acetic acid; Ambient temperature;
DOI:10.1016/S0040-4020(01)91538-8

Reference yield:

: 5539-66-2
1-hydroxy-8-methoxyanthraquinone

: 95636-48-9
1-hydroxy-8-methoxy-2-(1-oxo-2-sulfoxophenylpentyl)anthraquinone

Guidance literature:: Multi-step reaction with 9 steps

1: 87 percent / triphenylphosphine, diethyl-azodicarboxylate / tetrahydrofuran / 1 h / Ambient temperature

2: 87 percent / sodium dithionite / dimethylformamide; H₂O / 1) 70 deg C, 1 h 2) room temp., 1 h

3: RhCl₃*3H₂O / ethanol / 10 h / Heating

4: 93 percent / K₂CO₃ / acetone / 10 h / Heating

5: 79 percent / N-bromosuccinimide / acetone; H₂O / 0 °C

6: 94 percent / Jones reagent / acetone / Ambient temperature

7: 1) AlCl₃ / 1) CH₂Cl₂, overnight 2) overnight, HCl aq., THF

8: 90 percent / NaOH, cetyltrimethylammonium bromide / benzene; H₂O / 2.17 h

9: 85 percent / sodium metaperiodate / acetic acid; H₂O / Ambient temperature

With sodium hydroxide; sodium periodate; N-Bromosuccinimide; aluminium trichloride; sodium dithionite; jones reagent; cetyltrimethylammonim bromide; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; rhodium(III) chloride; In tetrahydrofuran; ethanol; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/S0040-4020(01)91538-8

Reference yield:

: 92908-99-1
1-methoxy-8-O-(1-penten-3-yl)anthraquinone

: 95636-48-9
1-hydroxy-8-methoxy-2-(1-oxo-2-sulfoxophenylpentyl)anthraquinone

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / sodium dithionite / dimethylformamide; H₂O / 1) 70 deg C, 1 h 2) room temp., 1 h

2: RhCl₃*3H₂O / ethanol / 10 h / Heating

3: 93 percent / K₂CO₃ / acetone / 10 h / Heating

4: 79 percent / N-bromosuccinimide / acetone; H₂O / 0 °C

5: 94 percent / Jones reagent / acetone / Ambient temperature

6: 1) AlCl₃ / 1) CH₂Cl₂, overnight 2) overnight, HCl aq., THF

7: 90 percent / NaOH, cetyltrimethylammonium bromide / benzene; H₂O / 2.17 h

8: 85 percent / sodium metaperiodate / acetic acid; H₂O / Ambient temperature

With sodium hydroxide; sodium periodate; N-Bromosuccinimide; aluminium trichloride; sodium dithionite; jones reagent; cetyltrimethylammonim bromide; potassium carbonate; rhodium(III) chloride; In ethanol; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/S0040-4020(01)91538-8