Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-
CAS No.:95730-73-7
Molecular Formula:C20H22O4
Molecular Weight:326.392
Hs Code.:

Synonyms:

Suppliers and Price of Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]-

There total 1 articles about Ethanone, 1-[3,4-dimethoxy-6-(phenylmethoxy)-2-(1-propenyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95730-73-7
6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)acetophenone

Guidance literature:: /BRN= 3312879/;

Reference yield: 85.0%

: 18871-63-1
3,3-ethylenedioxybutanal

: 95730-73-7
6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)acetophenone

: 95730-74-8
6'benzyloxy-3-hydroxy-3',4'-dimethoxy-4-(2-methyl-1,3-dioxolan-2-yl)-2'-(prop-1-enyl)butyrophenone

Guidance literature:: With magnesium; magnesium bromide; lithium diisopropyl amide; In tetrahydrofuran; -78 degC, 1 h then -78 degC, 3 h;
DOI:10.1039/P19870000389

Reference yield:

: 95730-73-7
6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)acetophenone

: 479-66-3
(-)-neurochromenin

Guidance literature:: Multi-step reaction with 12 steps

2: 1.) N-chlorosuccinimide, dimethyl sulphide, 2.) Zn / 2.) acetic acid

3: 87 percent / dioxane

4: sodium metaperiodate

5: 5percent H₂SO₄-AcOH / tetrahydrofuran / 3 h / Heating

7: 1.) H₂, 5percent HCl, 2.) O₃ / 1.) r.t., 4 d

8: 1.) O₃, 2.) Me₂S

9: sulphamic acid, sodium chlorite

10: H₂SO₄ / acetone

11: 52 percent / AlCl₃, Me₂S / CH₂Cl₂ / -10 °C

12: 68 percent / 5percent HCl / acetone / 24 h / 55 °C

With hydrogenchloride; sodium chlorite; sodium periodate; N-chloro-succinimide; aluminium trichloride; dimethylsulfide; sulfuric acid; aminosulfonic acid; hydrogen; ozone; acetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; acetone;
DOI:10.1039/c39840001565