Alpinigenin

Base Information

Chemical Name:Alpinigenin
CAS No.:14028-91-2
Molecular Formula:C22H27 N O6
Molecular Weight:401.45288
Hs Code.:
Mol file:14028-91-2.mol

Synonyms:Alpinigenine(8CI); Rheadan-8-ol, 2,3,10,11-tetramethoxy-16-methyl-, (6a,8a)-; Alpinigenin;[2]Benzopyrano[3,4-a][3]benzazepin-13-ol,4b,5,6,7,11b,13-hexahydro-1,2,9,10-tetramethoxy-5-methyl-, [4bR-(4ba,11bb,13b)]-

Suppliers and Price of Alpinigenin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Alpinigenin

Chemical Property:

Vapor Pressure:3.52E-12mmHg at 25°C
Boiling Point:532.8°Cat760mmHg
Flash Point:276°C
PSA：69.62000
Density:1.213g/cm³
LogP:2.95030

Purity/Quality:: 97.0% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Alpinigenin

There total 16 articles about Alpinigenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 1.0%

: 65022-58-4
N-(2-formyl-3,4-dimethoxybenzyl)-N-(2-formyl-4,5-dimethoxyphenethyl)methylamine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-cis-alpinigenine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-alpinigenine

Guidance literature:: In tert-butyl alcohol; at 37 ℃; for 3.5h; Irradiation;
DOI:10.1039/P19810001273

Reference yield: 1.0%

: 65022-58-4
N-(2-formyl-3,4-dimethoxybenzyl)-N-(2-formyl-4,5-dimethoxyphenethyl)methylamine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-cis-alpinigenine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-alpinigenine

Guidance literature:: In tert-butyl alcohol; at 37 ℃; for 3.5h; Irradiation;
DOI:10.1039/P19810001273

Reference yield:

: 64982-81-6
trans-1,2,10,11-tetramethoxy-6-methyl-5,6,7,8-tetrahydrodibenzazecine

: 14028-91-2,40163-61-9,40170-39-6,52745-32-1,78419-90-6,112459-13-9
(+/-)-cis-alpinigenine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1N hydrochloric acid, N-bromosuccinimide, 2.) 3N sodium hydroxide

2: 280 mg / 1N sulphuric acid, periodic acid / H₂O / 0.17 h

3: 30 percent / 2-methyl-propan-2-ol / 3.5 h / 37 °C / Irradiation

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; sulfuric acid; periodic acid; In water; tert-butyl alcohol;
DOI:10.1039/P19810001273