5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one

Base Information

Chemical Name:5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one
CAS No.:95793-09-2
Molecular Formula:C10H8N2O2
Molecular Weight:188.186
Hs Code.:
DSSTox Substance ID:DTXSID50538929
Wikidata:Q82414505
Mol file:95793-09-2.mol

Synonyms:5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one;95793-09-2;DTXSID50538929;5-methyl-2-phenyl-[1,3,4]oxadiazin-6-one

Suppliers and Price of 5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:188.058577502
Heavy Atom Count:14
Complexity:301

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NN=C(OC1=O)C2=CC=CC=C2

Technology Process of 5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one

There total 3 articles about 5-methyl-2-phenyl-6H-1,3,4-oxadiazin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 95793-10-5
syn-2-oxopropanoic acid benzoylhydrazone

: 95793-09-2
5-methyl-2-phenyl-1,3,4-oxadiazin-6-one

Guidance literature:: With dicyclohexyl-carbodiimide; In benzene; at 85 ℃; for 0.666667h;

Reference yield:

: 97509-69-8
anti-2-oxopropanoic acid benzoylhydrazone

: 95793-09-2
5-methyl-2-phenyl-1,3,4-oxadiazin-6-one

Guidance literature:: With dicyclohexyl-carbodiimide;
DOI:10.1016/S0040-4039(01)81607-5

Reference yield:

: 613-94-5
benzoic acid hydrazide

: 95793-09-2
5-methyl-2-phenyl-1,3,4-oxadiazin-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / H₂O / 2 h / 65 °C

2: 95 percent / p-toluenesulfonic acid / benzene / 4 h / Heating

3: 68 percent / dicyclohexylcarbodiimide / benzene / 0.67 h / 85 °C

With toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In water; benzene;