Technology Process of 1H-Pyrrole-3-carboxylic acid, 2,5-dimethyl-4-(4-methylphenyl)-, ethyl
ester
There total 3 articles about 1H-Pyrrole-3-carboxylic acid, 2,5-dimethyl-4-(4-methylphenyl)-, ethyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate; tetrabutylammonium tetrafluoroborate; water;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
Inert atmosphere;
Electrolysis;
DOI:10.1039/d1gc00487e
- Guidance literature:
-
With
hydrogenchloride; potassium hydroxide;
Yield given. Multistep reaction;
1) ether, reflux, 2) methanol, water, 0.5 h, reflux;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dipotassium peroxodisulfate / water; acetonitrile / 55 °C / Inert atmosphere
2: boron trifluoride diethyl etherate; tetrabutylammonium tetrafluoroborate; water / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere; Electrolysis
With
dipotassium peroxodisulfate; boron trifluoride diethyl etherate; tetrabutylammonium tetrafluoroborate; water;
In
tetrahydrofuran; water; acetonitrile;
DOI:10.1039/d1gc00487e
