Technology Process of 1H-Indene-1-methanamine,
2,3-dihydro-4,5-dimethoxy-N-(phenylmethyl)-, hydrochloride
There total 5 articles about 1H-Indene-1-methanamine,
2,3-dihydro-4,5-dimethoxy-N-(phenylmethyl)-, hydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ethereal hydrochloric acid; sodium acetate trihydrate; benzaldehyde;
platinum-on-carbon;
In
methanol; aqueous potassium hydroxide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: ZnI2 / benzene / 5 h / 60 °C
2: LiAlH4 / benzene; diethyl ether / 2 h / Heating
3: H2, 12 N aq. HCl / 10percent Pd/C / methanol / 20 h / Ambient temperature
4: H2, NaOAc*3H2O / 5percent Pt/C / methanol / 0.5 h / Ambient temperature
With
hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium acetate; zinc(II) iodide;
palladium on activated charcoal; platinum on activated charcoal;
In
methanol; diethyl ether; benzene;
DOI:10.1021/jm00148a005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2, 12 N aq. HCl / 10percent Pd/C / methanol / 20 h / Ambient temperature
2: H2, NaOAc*3H2O / 5percent Pt/C / methanol / 0.5 h / Ambient temperature
With
hydrogenchloride; hydrogen; sodium acetate;
palladium on activated charcoal; platinum on activated charcoal;
In
methanol;
DOI:10.1021/jm00148a005