Technology Process of Carbonic acid, 1,1-dimethylethyl 3-phenyl-2-propenyl ester, (E)-
There total 5 articles about Carbonic acid, 1,1-dimethylethyl 3-phenyl-2-propenyl ester, (E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(2E)-3-phenyl-2-propen-1-ol;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at 0 ℃;
for 0.166667h;
di-tert-butyl dicarbonate;
In
tetrahydrofuran; hexane;
at 0 - 20 ℃;
DOI:10.1021/ol203154j
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1135/cccc20080705
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / diethyl ether
2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / dichloromethane
With
tetra(n-butyl)ammonium hydrogensulfate; diisobutylaluminium hydride; sodium hydroxide;
In
diethyl ether; dichloromethane;
DOI:10.1021/jacs.6b11692
