4-((2-(2,4-Dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol

Base Information

• Chemical Name: 4-((2-(2,4-Dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol
• CAS No.: 36677-78-8
• Molecular Formula: C16H16N2O4
• Molecular Weight: 300.314
• NSC Number: 174252
• DSSTox Substance ID: DTXSID60420260
• Nikkaji Number: J1.121.010D,J3.499.127H
• Wikidata: Q82231489
• ChEMBL ID: CHEMBL374367

Synonyms:36677-78-8;CBDivE_005111;CHEMBL374367;4-((2-(2,4-dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol;4-[2-[(2,4-dihydroxyphenyl)methylideneamino]ethyliminomethyl]benzene-1,3-diol;N,N'-Bis(4-hydroxy salicylidene)ethylenediamine;SCHEMBL6833864;DTXSID60420260;BDBM50157740;NSC174252;ZINC01706667;NSC-174252;N,N'-bis(4-hydroxysalicylidene)ethylendiamine;N,N'-bis(4-hydroxysalicylidene) ethylenediamine

Chemical Property of 4-((2-(2,4-Dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol

Chemical Property:

• Boiling Point: 477.8°Cat760mmHg
• Flash Point: 242.7°C
• Density: 1.559g/cm³
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 300.11100700
• Heavy Atom Count: 22
• Complexity: 352

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1O)O)C=NCCN=CC2=C(C=C(C=C2)O)O

Technology Process of 4-((2-(2,4-Dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol

There total 2 articles about 4-((2-(2,4-Dihydroxybenzylideneamino)ethylimino)methyl)benzene-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

ethylenediamine (107-15-3,85404-18-8) + 2,4-Dihydroxybenzaldehyde (95-01-2) → N,N′-bis(2,4-dihydroxysalicylidene)ethylenediamine (36677-78-8)

Guidance literature:

In ethanol; for 6h; Inert atmosphere; Reflux; Schlenk technique;

DOI:10.1007/s11243-021-00447-7

Reference yield:

→ N,N′-bis(2,4-dihydroxysalicylidene)ethylenediamine (36677-78-8)

Guidance literature:

With acetic acid; In methanol; for 5h; Reflux;

Reference yield: 83.0%

N,N′-bis(2,4-dihydroxysalicylidene)ethylenediamine (36677-78-8) + nickel(II) acetate tetrahydrate (6018-89-9) → C16H14N2NiO4 (75931-17-8)

Guidance literature:

In ethanol; at 78 ℃; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1007/s11243-021-00447-7

upstream raw materials:

ethylenediamine

2,4-Dihydroxybenzaldehyde

Downstream raw materials:

4,4'-dihydroxysalen Mn(III) acetate

4,4'-dihydroxysalen Fe(III) chloride

Cu(HOC₆H₃(O)CHNCH₂CH₂NCHC₆H₃(O)OH)

(HOC₆H₃OCHN)2C₂H₄Ni

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