Technology Process of Benzoic acid, 4-[[6-(4-hydroxyphenoxy)hexyl]oxy]-
There total 9 articles about Benzoic acid, 4-[[6-(4-hydroxyphenoxy)hexyl]oxy]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
5%-palladium/activated carbon;
In
various solvent(s);
under 760 Torr;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / cyclohexanone / 6 h / Heating
2: 11.2 g / potassium hydroxide / ethanol; H2O / 6 h / Heating
3: 8.5 g / concentrated hydrochloric acid / H2O / 12 h / Ambient temperature
4: 1.4 g / hydrogen / Pd-5percent on charcoal / various solvent(s) / 760 Torr / Ambient temperature
With
hydrogenchloride; potassium hydroxide; hydrogen; potassium carbonate;
5%-palladium/activated carbon;
In
ethanol; water; cyclohexanone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 15.3 g / potassium carbonate / cyclohexanone / 4 h / Heating
2: 13 g / lithium aluminium hydride / diethyl ether / 4 h / Heating
3: 19.9 g / pyridine / 12 h / 0 °C
4: potassium carbonate / cyclohexanone / 6 h / Heating
5: 11.2 g / potassium hydroxide / ethanol; H2O / 6 h / Heating
6: 8.5 g / concentrated hydrochloric acid / H2O / 12 h / Ambient temperature
7: 1.4 g / hydrogen / Pd-5percent on charcoal / various solvent(s) / 760 Torr / Ambient temperature
With
pyridine; hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium carbonate;
5%-palladium/activated carbon;
In
diethyl ether; ethanol; water; cyclohexanone;
