4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one

Base Information

Chemical Name:4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one
CAS No.:96354-46-0
Molecular Formula:C11H12OS
Molecular Weight:192.282
Hs Code.:
DSSTox Substance ID:DTXSID00540779

Synonyms:96354-46-0;4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one;DTXSID00540779

Suppliers and Price of 4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:192.06088618
Heavy Atom Count:13
Complexity:226

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CS(=O)CC=C1C2=CC=CC=C2

Technology Process of 4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one

There total 1 articles about 4-Phenyl-3,6-dihydro-1lambda~4~-thiopyran-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 73813-60-2
4-phenyl-5,6-dihydro-2H-thiopyran

: 96354-46-0
4-phenyl-5,6-dihydro-2H-thiopyran 1-oxide

Guidance literature:: With sodium periodate; In methanol; water; for 6h;

Reference yield:

: 96354-46-0
4-phenyl-5,6-dihydro-2H-thiopyran 1-oxide

: 96354-48-2,96380-75-5
cis-2-methyl-4-phenyl-5,6-dihydro-2H-thiopyran 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C

2: 1.) triethyloxonium tetrafluoroborate, 2.) 0.3 M sodium hydroxide / 1.) CH₂Cl₂, from RT to 30 deg C, 1.5 h, 2.) CH₂Cl₂, H₂O, 2 h

With sodium hydroxide; triethyloxonium fluoroborate; lithium diisopropyl amide;