3-Furancarboxylic acid, tetrahydro-2-oxo-4-(phenylmethyl)-

Base Information

Chemical Name:3-Furancarboxylic acid, tetrahydro-2-oxo-4-(phenylmethyl)-
CAS No.:96540-42-0
Molecular Formula:C12H12O4
Molecular Weight:220.225
Hs Code.:

Synonyms:

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Chemical Property of 3-Furancarboxylic acid, tetrahydro-2-oxo-4-(phenylmethyl)-

Chemical Property:

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Technology Process of 3-Furancarboxylic acid, tetrahydro-2-oxo-4-(phenylmethyl)-

There total 5 articles about 3-Furancarboxylic acid, tetrahydro-2-oxo-4-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 96540-38-4
3-ethoxycarbonyl-4-benzyl-4,5-dihydrofuran-2(3H)-one

: 96540-42-0
3-carbonyl-4-benzyl-4,5-dihydrofuran-2(3H)-one

Guidance literature:: With sodium hydroxide; In ethanol; water; for 1h; Ambient temperature;

Reference yield:

: 96540-63-5
cinnamyl ethyl malonate

: 96540-42-0
3-carbonyl-4-benzyl-4,5-dihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / tosyl azide, triethylamine / acetonitrile / 3 h / Ambient temperature

2: 67 percent / Rh₂(OAc)4 / benzene / 1 h / Heating

3: 60 percent / trimethylsilyl chloride, sodium iodide / acetonitrile / 15 h / Ambient temperature

4: 78 percent / tri-n-butyltin hydride, α,α-azobisisobutyronitrile / tetrahydrofuran / 1 h / Heating

5: 90 percent / 0.25N NaOH / ethanol; H₂O / 1 h / Ambient temperature

With dirhodium tetraacetate; sodium hydroxide; chloro-trimethyl-silane; 4-toluenesulfonyl azide; azobisisobutyronitrile; tri-n-butyl-tin hydride; triethylamine; sodium iodide; In tetrahydrofuran; ethanol; water; acetonitrile; benzene;

Reference yield:

: 96540-32-8
1-ethoxycarbonyl-3-oxa-2-oxo-6-phenylbicyclo<3.1.0>hexane

: 96540-42-0
3-carbonyl-4-benzyl-4,5-dihydrofuran-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / trimethylsilyl chloride, sodium iodide / acetonitrile / 15 h / Ambient temperature

2: 78 percent / tri-n-butyltin hydride, α,α-azobisisobutyronitrile / tetrahydrofuran / 1 h / Heating

3: 90 percent / 0.25N NaOH / ethanol; H₂O / 1 h / Ambient temperature

With sodium hydroxide; chloro-trimethyl-silane; azobisisobutyronitrile; tri-n-butyl-tin hydride; sodium iodide; In tetrahydrofuran; ethanol; water; acetonitrile;