2-Propenoic acid, 2-hydroxy-3-[2-nitro-3-(phenylmethoxy)phenyl]-, ethyl ester, potassium salt

Base Information

Chemical Name:2-Propenoic acid, 2-hydroxy-3-[2-nitro-3-(phenylmethoxy)phenyl]-, ethyl ester, potassium salt
CAS No.:96564-49-7
Molecular Formula:C18H17NO6.K
Molecular Weight:381.426
Hs Code.:

Synonyms:

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Chemical Property of 2-Propenoic acid, 2-hydroxy-3-[2-nitro-3-(phenylmethoxy)phenyl]-, ethyl ester, potassium salt

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Technology Process of 2-Propenoic acid, 2-hydroxy-3-[2-nitro-3-(phenylmethoxy)phenyl]-, ethyl ester, potassium salt

There total 3 articles about 2-Propenoic acid, 2-hydroxy-3-[2-nitro-3-(phenylmethoxy)phenyl]-, ethyl ester, potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 61535-21-5
1-(benzyloxy)-3-methyl-2-nitrobenzene

: 95-92-1
oxalic acid diethyl ester

: 96564-49-7
ethyl 3-(3-benzyloxy-2-nitrophenyl)-pyruvate, potassium salt

Guidance literature:: With potassium ethoxide; In diethyl ether; for 20h; Heating;

Reference yield:

: 4920-77-8
3-methyl-2-nitrophenol

: 96564-49-7
C₁₈H₁₆NO₆^(1-)*K⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 2.5 h / 75 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran; tert-butyl methyl ether / 24 h / Inert atmosphere; Heating

With potassium tert-butylate; potassium carbonate; In tetrahydrofuran; tert-butyl methyl ether; acetonitrile;
DOI:10.1271/bbb.100124

Reference yield:

: 61535-21-5
1-(benzyloxy)-3-methyl-2-nitrobenzene

: 95-92-1
oxalic acid diethyl ester

: 96564-49-7
C₁₈H₁₆NO₆^(1-)*K⁽¹⁺⁾

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; tert-butyl methyl ether; for 24h; Inert atmosphere; Heating;
DOI:10.1271/bbb.100124