Spiro[1H-indene-1,4'-piperidine], 2,3-dihydro-, hydrochloride

Base Information

• Chemical Name: Spiro[1H-indene-1,4'-piperidine], 2,3-dihydro-, hydrochloride
• CAS No.: 96651-85-3
• Molecular Formula: C13H17N.ClH
• Molecular Weight: 223.746
• Hs Code.: 2933399090
• Mol file: 96651-85-3.mol

Synonyms:2,3-Dihydrospiro[1H-indene-1,4'-piperidine]Hydrochloride;2,3-dihydrospiro[indene-1,4'-piperidine] hydrochloride;Spiro[indane-1,4'-piperidine] HCl;spiro[indane-1,4'-piperidine] hydrochloride;3,4-dihydrospiro(1H-indene-1,4'-piperidine) hydrochloride;Spiroindanepiperidinehydrochloride;2,3-dihydrospiro[indene-1,4'-piperidinium] chloride;4-Spiroindane-piperidine hydrochloride;

Chemical Property of Spiro[1H-indene-1,4'-piperidine], 2,3-dihydro-, hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 3.38480

Purity/Quality:

98%min ^*data from raw suppliers

2,3-Dihydrospiro[indene-1,4''-piperidine]Hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,3-Dihydrospiro[indene-1,4'-piperidine] hydrochloride is a useful research chemical.

Technology Process of Spiro[1H-indene-1,4'-piperidine], 2,3-dihydro-, hydrochloride

There total 2 articles about Spiro[1H-indene-1,4'-piperidine], 2,3-dihydro-, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

spiro(1H-indene-1,4'-piperidine) hydrochloride (137730-67-7) → 2,3-dihydrospiro[1H-indene-1,4'-piperidine] hydrochloride (96651-85-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 1h; under 2585.7 Torr;

DOI:10.1021/jm00089a013

Reference yield:

1'-(tert-butyloxycarbonyl)spiro<1H-indene-1,4'-piperidine> (137419-24-0) + spiro(1H-indene-1,4'-piperidine) hydrochloride (137730-67-7) → 2,3-dihydrospiro[1H-indene-1,4'-piperidine] hydrochloride (96651-85-3)

Guidance literature:

With hydrogenchloride; In ethanol; palladium; ethyl acetate;

Reference yield: 41.0%

2-[(4-bromophenyl)methyl]oxirane (62826-21-5) + 2,3-dihydrospiro[1H-indene-1,4'-piperidine] hydrochloride (96651-85-3) → 2,3-dihydro-1'-[3-(4-bromophenyl)-2-hydroxypropan-1-yl]spiro[1H-indene-1,4'-piperidine]

Guidance literature:

With potassium carbonate; In ethanol; for 21h; Heating;

DOI:10.1021/jm970326r

upstream raw materials:

spiro(1H-indene-1,4'-piperidine) hydrochloride

1'-(tert-butyloxycarbonyl)spiro<1H-indene-1,4'-piperidine>

Downstream raw materials:

N-[1(R)-[(2,3-dihydrospiro[1H-indene-1,4'-piperidin]-1'-yl)carbonyl]-2-(phenylmethyloxy)ethyl]carbamic acid 1,1-dimethylethyl ester

N-[1 (S)-[(2,3-dihydrospiro[1H-indene-1,4'-piperidin]-1'-yl)carbonyl]-2-(phenylmethylthio)ethyl]carbamic acid 1,1-dimethylethyl ester

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