TIMTEC-BB SBB009879

Base Information

Chemical Name:TIMTEC-BB SBB009879
CAS No.:96656-49-4
Molecular Formula:C12H9N3O3
Molecular Weight:243.222
Hs Code.:
Mol file:96656-49-4.mol

Synonyms:2-nitro-N-(2-pyridyl)benzamide;2-nitro-N-(pyridin-2-yl)benzamide;2-nitro-benz(2-pyridyl)amide;2-Nitro-N-pyridin-2-yl-benzamide;

Suppliers and Price of TIMTEC-BB SBB009879

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Nitro-N-(pyridin-2-yl)benzamide 97%
10g
$ 424.00

Crysdot
2-Nitro-N-(pyridin-2-yl)benzamide 97%
5g
$ 306.00

Total 4 raw suppliers

Chemical Property of TIMTEC-BB SBB009879

Chemical Property:

Melting Point:166 - 168 °C
PSA：87.81000
LogP:2.83830

Purity/Quality:

99% ^*data from raw suppliers

2-Nitro-N-(pyridin-2-yl)benzamide 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xn
Statements: 22

MSDS Files:

Useful:

Technology Process of TIMTEC-BB SBB009879

There total 3 articles about TIMTEC-BB SBB009879 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 504-29-0
2-aminopyridine

: 552-89-6
2-nitro-benzaldehyde

: 96656-49-4
2-nitro-N-(pyridine-2-yl)benzamide

Guidance literature:: With tert.-butylhydroperoxide; copper(l) iodide; In water; at 20 ℃; for 6h;
DOI:10.1016/j.cclet.2017.03.008

Reference yield: 81.0%

: 504-29-0
2-aminopyridine

: 610-14-0
2-nitrobenzyl chloride

: 96656-49-4
2-nitro-N-(pyridine-2-yl)benzamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 96656-49-4
2-nitro-N-(pyridine-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 6 h / Reflux

2: triethylamine / tetrahydrofuran / 0 °C

With thionyl chloride; triethylamine; In tetrahydrofuran;