Phenol, 2,6-dichloro-3-methoxy-5-methyl-

Base Information

Chemical Name:Phenol, 2,6-dichloro-3-methoxy-5-methyl-
CAS No.:96682-22-3
Molecular Formula:C8H8Cl2O2
Molecular Weight:207.056
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2,6-dichloro-3-methoxy-5-methyl-

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Technology Process of Phenol, 2,6-dichloro-3-methoxy-5-methyl-

There total 14 articles about Phenol, 2,6-dichloro-3-methoxy-5-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 4101-80-8
dichloroisoeverninic acid

: 96682-22-3
2,4-dichloro-3-hydroxy-5-methoxy-toluene

Guidance literature:: With sodium hydroxide; In water; for 168h; Heating;

Reference yield:

: 22375-05-9
methyl 4-benzyloxy-2-hydroxy-6-methylbenzoate

: 96682-22-3
2,4-dichloro-3-hydroxy-5-methoxy-toluene

Guidance literature:: Multi-step reaction with 5 steps

1: 74.2 percent / 4 mol Cl₂, NaOAc / acetic acid / 1.67 h / 20 °C

2: 88 percent / diethyl ether / 18 h / 0 °C

3: 99 percent / potassium t-butylate / H₂O; diethyl ether / 336 h / 20 °C

4: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h / 900.07 Torr

5: pyridine-d5 / 336 h / 20 °C

With potassium tert-butylate; hydrogen; sodium acetate; chlorine; palladium on activated charcoal; In perdeuteriopyridine; diethyl ether; water; acetic acid; ethyl acetate;
DOI:10.1016/S0040-4020(01)83482-7

Reference yield:

: 39803-55-9
4-Benzyloxy-3,5-dichloro-2-hydroxy-6-methyl-benzoic acid methyl ester

: 96682-22-3
2,4-dichloro-3-hydroxy-5-methoxy-toluene

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / diethyl ether / 18 h / 0 °C

2: 99 percent / potassium t-butylate / H₂O; diethyl ether / 336 h / 20 °C

3: 88 percent / H₂ / 10percent Pd/C / ethyl acetate / 3 h / 900.07 Torr

4: pyridine-d5 / 336 h / 20 °C

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In perdeuteriopyridine; diethyl ether; water; ethyl acetate;
DOI:10.1016/S0040-4020(01)83482-7