Benzamide, N,N-diethyl-2,6-diiodo-

Base Information

Chemical Name:Benzamide, N,N-diethyl-2,6-diiodo-
CAS No.:97567-50-5
Molecular Formula:C11H13I2NO
Molecular Weight:429.039
Hs Code.:
DSSTox Substance ID:DTXSID00446262
Wikidata:Q82264874

Synonyms:Benzamide, N,N-diethyl-2,6-diiodo-;97567-50-5;DTXSID00446262

Suppliers and Price of Benzamide, N,N-diethyl-2,6-diiodo-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, N,N-diethyl-2,6-diiodo-

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:428.90866
Heavy Atom Count:15
Complexity:209

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=C(C=CC=C1I)I

Technology Process of Benzamide, N,N-diethyl-2,6-diiodo-

There total 3 articles about Benzamide, N,N-diethyl-2,6-diiodo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 85370-72-5
2,6-dibromo-N,N-diethylbenzamide

: 97567-50-5
2,6-diiodo-N,N-diethylbenzamide

Guidance literature:: With iodine; tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1016/S0040-4039(00)98418-1

Reference yield:

: 1696-17-9
N,N-diethylbenzamide

: 74-88-4
methyl iodide

: 2728-04-3
N,N-diethyl-ortho-toluamide

: 57806-77-6
1-(N,N-diethylcarbamoyl)-2,6-dimethylbenzene

: 97567-50-5
2,6-diiodo-N,N-diethylbenzamide

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00247a013

Reference yield:

: 1696-17-9
N,N-diethylbenzamide

: 97567-50-5
2,6-diiodo-N,N-diethylbenzamide

Guidance literature:: With 2,2,6,6-tetramethylpiperidinyl-lithium; iodine; mercury dichloride; Yield given. Multistep reaction; 1.) THF, hexane, 1 h, 20 deg C;
DOI:10.1021/jo00247a013