1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene

Base Information

Chemical Name:1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene
CAS No.:97818-84-3
Molecular Formula:C24H23ClO
Molecular Weight:362.899
Hs Code.:
DSSTox Substance ID:DTXSID901186309

Synonyms:DTXSID901186309;1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene;97818-84-3

Suppliers and Price of 1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene

Chemical Property:

XLogP3:7.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:362.1437430
Heavy Atom Count:26
Complexity:424

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(=C(C1=CC=CC=C1)C2=CC=C(C=C2)OCCCl)C3=CC=CC=C3
Isomeric SMILES:CC/C(=C(/C1=CC=CC=C1)\C2=CC=C(C=C2)OCCCl)/C3=CC=CC=C3

Technology Process of 1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene

There total 21 articles about 1-(2-Chloroethoxy)-4-[(1E)-1,2-diphenyl-1-buten-1-yl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 28557-00-8
phenylzinc chloride

: 129920-99-6
(E)-1-bromo-1-<4-(2-chloroethoxy)phenyl>-2-phenyl-1-butene

: 97818-83-2
(Z)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

: 97818-84-3
(E)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 1h; Product distribution; other catalyst, solvent, and reaction temperature;
DOI:10.1021/jo00312a027

Reference yield: 98.0%

: 129920-99-6
(E)-1-bromo-1-<4-(2-chloroethoxy)phenyl>-2-phenyl-1-butene

: phenylmagnesium chloride

: 97818-83-2
(Z)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

: 97818-84-3
(E)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 1h; Product distribution; other catalyst, solvent, reaction temperature and time;
DOI:10.1021/jo00312a027

Reference yield: 96.0%

: 960-16-7
tributylphenylstannane

: 129920-99-6
(E)-1-bromo-1-<4-(2-chloroethoxy)phenyl>-2-phenyl-1-butene

: 97818-83-2
(Z)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

: 97818-84-3
(E)-1-<4-(2-chloroethoxy)phenyl>-1,2-diphenyl-1-butene

Guidance literature:: With lithium bromide; bis(η3-allyl-μ-chloropalladium(II)); In N,N,N,N,N,N-hexamethylphosphoric triamide; at 25 ℃; for 24h; Product distribution; other solvent;
DOI:10.1021/jo00312a027