ADAMANTANE-1-CARBOHYDRAZIDE

Base Information

• Chemical Name: ADAMANTANE-1-CARBOHYDRAZIDE
• CAS No.: 17846-15-0
• Molecular Formula: C11H18 N2 O
• Molecular Weight: 194.277
• Hs Code.: 2928000090
• Mol file: 17846-15-0.mol

Synonyms:1-Adamantanecarboxylicacid, hydrazide (6CI,8CI); 1-Adamantylcarboxylic acid hydrazide; NSC 354302

Chemical Property of ADAMANTANE-1-CARBOHYDRAZIDE

Chemical Property:

• Vapor Pressure: 1.08E-05mmHg at 25°C
• Melting Point: 151 °C
• Boiling Point: 370.8°Cat760mmHg
• PKA: 13.71±0.20(Predicted)
• Flash Point: 178°C
• PSA: 55.12000
• Density: 1.203g/cm³
• LogP: 2.28390

Purity/Quality:

97% ^*data from raw suppliers

Adamantane-1-carbohydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): R36/37/38:Irritating to eyes, respiratory system and skin.
• Hazard Codes: Xi:Irritant
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ADAMANTANE-1-CARBOHYDRAZIDE

There total 6 articles about ADAMANTANE-1-CARBOHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

methyl adamantane-1-carboxylate (711-01-3) → adamantane-1-carbohydrazide (17846-15-0)

Guidance literature:

With hydrazine; In ethanol; at 120 ℃; Microwave irradiation;

DOI:10.2174/15701786113106660063

Reference yield: 81.0%

ethyl 1-adamantanecarboxylate (2094-73-7) → adamantane-1-carbohydrazide (17846-15-0)

Guidance literature:

With hydrazine hydrate; In ethanol; at 150 - 160 ℃; for 144h; Autoclave; High pressure;

DOI:10.1002/cmdc.201900165

Reference yield: 78.0%

1-Adamantanecarboxylic acid (828-51-3) → adamantane-1-carbohydrazide (17846-15-0)

Guidance literature:

1-Adamantanecarboxylic acid; With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

With hydrazine hydrate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

DOI:10.1111/cbdd.13836

upstream raw materials:

ethyl 1-adamantanecarboxylate

ethyl 2-(1-adamantylcarbonyl)-3-oxobutanoate

methyl adamantane-1-carboxylate

1-Adamantanecarboxylic acid

Downstream raw materials:

1-(1-adamantylcarbonyl)-4-benzylthiosemicarbazide

2-adamantane-1-carbonyl N-phenylhydrazine carbothioamide

1-(1-adamantylcarbonyl)-4-(4-chlorophenyl)thiosemicarbazide

C₁₇H₂₂N₂O₃S

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