1,2-Bis(2-chloroethoxy)-4-nitrobenzene

Base Information

Chemical Name:1,2-Bis(2-chloroethoxy)-4-nitrobenzene
CAS No.:97916-49-9
Molecular Formula:C10H11Cl2NO4
Molecular Weight:280.108
Hs Code.:
European Community (EC) Number:635-543-8
DSSTox Substance ID:DTXSID50367973
Wikidata:Q82154208

Synonyms:1,2-bis(2-chloroethoxy)-4-nitrobenzene;97916-49-9;Benzene, 1,2-bis(2-chloroethoxy)-4-nitro-;SCHEMBL9220403;DTXSID50367973;HYZDQDAVZVEVKU-UHFFFAOYSA-N;STL089752;AKOS000519768;1,2-Bis-(2-chloroethoxy)-4-nitrobenzene;Z56755933

Suppliers and Price of 1,2-Bis(2-chloroethoxy)-4-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,2-BIS-(2-CHLORO-ETHOXY)-4-NITRO-BENZENE 95.00%
5MG
$ 495.50

Total 0 raw suppliers

Chemical Property of 1,2-Bis(2-chloroethoxy)-4-nitrobenzene

Chemical Property:

Boiling Point:420.1±35.0 °C(Predicted)
PSA：64.28000
Density:1.365±0.06 g/cm3(Predicted)
LogP:3.35320
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:279.0065132
Heavy Atom Count:17
Complexity:237

Purity/Quality:: 1,2-BIS-(2-CHLORO-ETHOXY)-4-NITRO-BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1[N+](=O)[O-])OCCCl)OCCCl

Technology Process of 1,2-Bis(2-chloroethoxy)-4-nitrobenzene

There total 4 articles about 1,2-Bis(2-chloroethoxy)-4-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 83257-95-8
1,2-di(2-hydroxyethoxy)-4-nitrobenzene

: 97916-49-9
4-nitro-1,2-bis(2-chloroethoxy)benzene

Guidance literature:: With pyridine; thionyl chloride; In toluene;

Reference yield: 74.0%

: 53219-99-1
1,2-bis(1'-chloro-2'-ethoxy)benzene

: 97916-49-9
4-nitro-1,2-bis(2-chloroethoxy)benzene

Guidance literature:: With nitric acid;
DOI:10.1007/BF02253174

Reference yield:

: 3316-09-4
1,2-dihydroxy-4-nitrobenzene

: 97916-49-9
4-nitro-1,2-bis(2-chloroethoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 3 h / Heating / reflux

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h

3: pyridine; thionyl chloride / toluene / 1 h / Heating / reflux

With pyridine; sodium tetrahydroborate; thionyl chloride; potassium carbonate; In tetrahydrofuran; methanol; acetone; toluene;