Pyridazino[4,3-c]isoquinoline, 5,6-dihydro-3-phenyl-

Base Information

Chemical Name:Pyridazino[4,3-c]isoquinoline, 5,6-dihydro-3-phenyl-
CAS No.:98045-93-3
Molecular Formula:C17H13N3
Molecular Weight:259.31
Hs Code.:

Synonyms:

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Chemical Property of Pyridazino[4,3-c]isoquinoline, 5,6-dihydro-3-phenyl-

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Technology Process of Pyridazino[4,3-c]isoquinoline, 5,6-dihydro-3-phenyl-

There total 4 articles about Pyridazino[4,3-c]isoquinoline, 5,6-dihydro-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 96825-78-4
6-Chloro-3-phenyl-pyridazino-[4,3-c]-isoquinoline

: 98045-93-3
5,6-dihydro-3-phenylpyridazino<4,3-c>isoquinoline

Guidance literature:: With hydrogen; palladium on activated charcoal; magnesium oxide; In 2-methoxy-ethanol; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00147a034

Reference yield:

: 96825-74-0
3-phenyl-pyridazino [4,3-c]isoquinolin-6-(5H)-one

: 98045-93-3
5,6-dihydro-3-phenylpyridazino<4,3-c>isoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / phosphorus pentachloride, phosphorus oxychloride / 3.5 h / Heating

2: 74 percent / H₂ / 10percent Pd/C, magnesium oxide / 2-methoxy-ethanol / 760 Torr / Ambient temperature

With phosphorus pentachloride; hydrogen; trichlorophosphate; palladium on activated charcoal; magnesium oxide; In 2-methoxy-ethanol;
DOI:10.1021/jm00147a034

Reference yield:

: 73351-33-4
2-(4-oxo-6-phenyl-1,4-dihydro-pyridazin-3-yl)-benzoic acid

: 98045-93-3
5,6-dihydro-3-phenylpyridazino<4,3-c>isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: acetic anhydride / toluene / 1.5 h / Heating

2: ammonium acetate / 9 h / 190 - 200 °C

3: 94 percent / phosphorus pentachloride, phosphorus oxychloride / 3.5 h / Heating

4: 74 percent / H₂ / 10percent Pd/C, magnesium oxide / 2-methoxy-ethanol / 760 Torr / Ambient temperature

With ammonium acetate; phosphorus pentachloride; hydrogen; acetic anhydride; trichlorophosphate; palladium on activated charcoal; magnesium oxide; In 2-methoxy-ethanol; toluene;
DOI:10.1021/jm00147a034