Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate

Base Information

Chemical Name:Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate
CAS No.:98236-89-6
Molecular Formula:C₁₃H₁₄N₂O₅
Molecular Weight:278.265
Hs Code.:
DSSTox Substance ID:DTXSID10540083

Synonyms:98236-89-6;Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate;DTXSID10540083

Suppliers and Price of Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:278.09027155
Heavy Atom Count:20
Complexity:395

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)N(C1=CC=CC=C1)N=C(C(=O)OC)C(=O)OC

Technology Process of Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate

There total 1 articles about Dimethyl (2-acetyl-2-phenylhydrazinylidene)propanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 3298-40-6
mesoxalate de methyle

: 2116-41-8
1-Acetyl-1-phenylhydrazin

: 98236-89-6
dimethyl mesoxalate N-acetyl-N-phenylhydrazone

Guidance literature:: In toluene; Heating;

Reference yield: 92.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 98236-89-6
dimethyl mesoxalate N-acetyl-N-phenylhydrazone

: 98236-90-9
dimethyl 1-(N-acetyl-N-phenylamino)-Δ²-1,2,3-triazoline-5,5-dicarboxylate

Guidance literature:: In diethyl ether; chloroform; for 120h;

Reference yield:

: 98236-89-6
dimethyl mesoxalate N-acetyl-N-phenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CHCl₃; diethyl ether / 120 h

2: 42 percent / trifluoroacetic acid / CHCl₃ / 4 h / 0 °C

With trifluoroacetic acid; In diethyl ether; chloroform;