5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde

Base Information

Chemical Name:5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde
CAS No.:99066-69-0
Molecular Formula:C9H6N2OS
Molecular Weight:190.225
Hs Code.:
European Community (EC) Number:822-253-3
DSSTox Substance ID:DTXSID70566002
Wikidata:Q82451403

Synonyms:5-PHENYL-1,3,4-THIADIAZOLE-2-CARBALDEHYDE;99066-69-0;1,3,4-Thiadiazole-2-carboxaldehyde, 5-phenyl-;SCHEMBL10972611;DTXSID70566002;AB72803;EN300-1706976;Z1255405945

Suppliers and Price of 5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:190.02008399
Heavy Atom Count:13
Complexity:183

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NN=C(S2)C=O

Technology Process of 5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde

There total 5 articles about 5-Phenyl-1,3,4-thiadiazole-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 121564-79-2
2-Azidomethyl-5-phenyl-[1,3,4]thiadiazole

: 99066-69-0
5-phenyl-1,3, 4-thiadiazole-2-carbaldehyde

Guidance literature:: With sulfuric acid; at 0 - 12 ℃; for 24h;

Reference yield: 73.5%

: (5-Phenyl-1,3,4-thiadiazol-2-yl)methanol

: 99066-69-0
5-phenyl-1,3, 4-thiadiazole-2-carbaldehyde

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1456-72-0
2-methyl-5-phenyl-1,3,4-thiadiazole

: 99066-69-0
5-phenyl-1,3, 4-thiadiazole-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl₄ / 50 °C

2: 81 percent / sodium azide, sodium iodide / Ambient temperature

3: 82 percent / conc. sulfuric acid / 24 h / 0 - 12 °C

With N-Bromosuccinimide; sodium azide; sulfuric acid; sodium iodide; dibenzoyl peroxide; In tetrachloromethane;