2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester

Base Information

Chemical Name:2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester
CAS No.:99303-73-8
Molecular Formula:C20H16O4
Molecular Weight:320.33900
Hs Code.:

Synonyms:1-phenyl-2-methoxycarbonyl-4-acetoxy-naphthalene;1-phenyl-2-methoxycarbonyl-4-acetoxy-naphthaline;

Suppliers and Price of 2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester

Chemical Property:

PSA：52.60000
LogP:4.21870

Purity/Quality:: 99.3% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester

There total 3 articles about 2-Naphthalenecarboxylic acid, 4-(acetyloxy)-1-phenyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108-24-7
acetic anhydride

: 23242-84-4
3-Carbomethoxy-4,4-diphenyl-3-butenoic acid

: 99303-73-8
methyl ester of 4-acetoxy-1-phenyl-2-naphthoic acid

Guidance literature:: In toluene; for 16h; Inert atmosphere; Reflux;

Reference yield:

: 119-61-9
benzophenone

: 108-24-7
acetic anhydride

: 106-65-0
Dimethyl succinate

: 99303-73-8
methyl ester of 4-acetoxy-1-phenyl-2-naphthoic acid

Guidance literature:: Dimethyl succinate; With methanol; sodium hydride; In hexane; toluene; mineral oil; at 0 ℃; for 0.25h; Inert atmosphere;

benzophenone; In hexane; toluene; mineral oil; at 0 - 20 ℃; Inert atmosphere;

acetic anhydride; With sodium acetate; at 0 ℃; Reflux;
DOI:10.1021/acs.joc.5b01251