2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Base Information

Chemical Name:2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI)
CAS No.:142762-73-0
Molecular Formula:C38H54 N8 O6 S2
Molecular Weight:783.0154
Hs Code.:

2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Synonyms:2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, [2R-[2a(R*),4b[2'R*(R*),4'S*]]]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

Chemical Property:

Boiling Point:1171.9oC at 760 mmHg
Flash Point:662.6oC
PSA：270.20000
Density:1.213g/cm3
LogP:6.26480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI)

There total 5 articles about 2-Thiazolidineacetamide,4,4'-[1,2-ethanediylbis(iminocarbonyl)]bis[N-ethyl-5,5-dimethyl-a-[(phenylacetyl)amino]-, (aR,a'R,2R,2'R,4S,4'S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.4%

: 75-04-7,85404-22-4
ethylamine

: 142762-72-9
<2S-<2α,5α,6β>>-N,N'-<1,2-ethanediyl>bis<3,3-dimethyl-7-oxo-6-<(phenylacetyl)amino>-4-thia-1-azabicyclo<3.2.0>heptane-2-carboxamide>

: 142762-73-0
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[N-ethyl-5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetamide]

Guidance literature:: In dichloromethane; at 0 - 5 ℃; for 60h;
DOI:10.1021/jm00073a011

Reference yield:

: 39879-63-5
penicillin-G N-ethylpiperidine salt

: 142762-73-0
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[N-ethyl-5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetamide]

Guidance literature:: Multi-step reaction with 3 steps

1: CHCl₃ / 2 h / -11 °C

2: CHCl₃ / 2 h / 0 - 19 °C

3: 69.4 percent / CH₂Cl₂ / 60 h / 0 - 5 °C

In dichloromethane; chloroform;
DOI:10.1021/jm00073a011

Reference yield:

: 19870-47-4
benzylpenicillin-(carbonic acid ethyl ester)-anhydride

: 142762-73-0
[2R-(2α(R^*),4β)]-4,4'-[1,2-ethanediylbis(aminocarbonyl)]bis[N-ethyl-5,5-dimethyl-α-[(phenylacetyl)amino]-2-thiazolidineacetamide]

Guidance literature:: Multi-step reaction with 2 steps

1: CHCl₃ / 2 h / 0 - 19 °C

2: 69.4 percent / CH₂Cl₂ / 60 h / 0 - 5 °C

In dichloromethane; chloroform;
DOI:10.1021/jm00073a011