Benzenepropanal, 2-acetyl-

Base Information

Chemical Name:Benzenepropanal, 2-acetyl-
CAS No.:99865-14-2
Molecular Formula:C11H12O2
Molecular Weight:176.21200
Hs Code.:
Mol file:99865-14-2.mol

Synonyms:2-Acetyl-hydrozimtaldehyd;3-<2-Acetamino-ethyl>-6-hydroxy-5-methoxy-indol;6-hydroxy-melatonin;Lopac-H-0627;

Suppliers and Price of Benzenepropanal, 2-acetyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Benzenepropanal, 2-acetyl-

Chemical Property:

Vapor Pressure:0.002mmHg at 25°C
Boiling Point:291.953oC at 760 mmHg
Flash Point:108.852oC
PSA：34.14000
Density:1.051g/cm3
LogP:2.02070

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Technology Process of Benzenepropanal, 2-acetyl-

There total 8 articles about Benzenepropanal, 2-acetyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1-methyl-1,2,3,4-tetrahydronaphthalene-1,2-diol

: 99865-14-2
3-(2-acetylphenyl)propanal

Guidance literature:: With [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/c6ob01203e

Reference yield: 35.0%

: 4373-13-1
4-methyl-1,2-dihydronaphthalene

: 99865-14-2
3-(2-acetylphenyl)propanal

Guidance literature:: 4-methyl-1,2-dihydronaphthalene; With ozone; In methanol; at -78 ℃; for 4h;

With dimethylsulfide; In methanol; at 20 ℃; for 24h;
DOI:10.1055/s-0030-1260320

Reference yield:

: 200425-59-8
(S)-(+)-1-methyl-1,2,3,4-tetrahydronaphthalen-1-ol

: 99865-14-2
3-(2-acetylphenyl)propanal

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 18 h / 60 °C

2: potassium carbonate / methanol / 0.5 h / 0 °C

3: [bis(acetoxy)iodo]benzene / dichloromethane / 1 h / 20 °C

With [bis(acetoxy)iodo]benzene; potassium carbonate; acetic acid; In methanol; dichloromethane;
DOI:10.1039/c6ob01203e