2-NITRO-6(5H)-PHENANTHRIDINONE

Base Information

• Chemical Name: 2-NITRO-6(5H)-PHENANTHRIDINONE
• CAS No.: 78256-30-1
• Molecular Formula: C13H8 N2 O3
• Molecular Weight: 240.218
• Hs Code.: 2933990090
• Mol file: 78256-30-1.mol

Synonyms:2-Nitro-6(5H)-phenanthridinone;NSC 113304; PJ 97B

Chemical Property of 2-NITRO-6(5H)-PHENANTHRIDINONE

Chemical Property:

• Vapor Pressure: 2.22E-05mmHg at 25°C
• Boiling Point: 360.4°C at 760 mmHg
• Flash Point: 171.8°C
• PSA: 78.68000
• Density: 1.409g/cm³
• LogP: 3.11270

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-NITRO-6(5H)-PHENANTHRIDINONE

There total 22 articles about 2-NITRO-6(5H)-PHENANTHRIDINONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

6(5H)-phenanthridinone (1015-89-0) → 2-nitrophenanthridin-6(5H)-one (78256-30-1)

Guidance literature:

With nitric acid; acetic acid; at 100 ℃; for 2h;

DOI:10.1021/acs.orglett.9b01105

Reference yield: 75.5%

6(5H)-phenanthridinone (1015-89-0) → 2-nitrophenanthridin-6(5H)-one (78256-30-1) + 4-nitro-6(5H)-phenanthridinone (23818-43-1)

Guidance literature:

With nitric acid; acetic acid; for 2h; Product distribution; Heating;

DOI:10.1007/BF00519824

Reference yield: 27.0%

6-chlorophenanthridine (15679-03-5) → 2-nitrophenanthridin-6(5H)-one (78256-30-1) + 4-nitro-6(5H)-phenanthridinone (23818-43-1)

Guidance literature:

With silver nitrate; In acetonitrile; for 0.5h;

upstream raw materials:

6-methyl-2-nitro-phenanthridine

3-nitro-9H-fluoren-9-one

6(5H)-phenanthridinone

6-chlorophenanthridine

Downstream raw materials:

2-aminophenanthridin-6(5H)-one

2-nitro-N-[4-methylphenyl]sulfonyl-5,6-dihydrophenanthridine

2-nitro-6-chlorophenanthridine

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