5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine

Base Information

• Chemical Name: 5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine
• CAS No.: 129015-69-6
• Molecular Formula: C6H5ClF3N3
• Molecular Weight: 211.57
• Hs Code.: 2933990090
• DSSTox Substance ID: DTXSID50369432
• Wikidata: Q82156505
• Mol file: 129015-69-6.mol

Synonyms:5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine;129015-69-6;1-[5-chloro-3-(trifluoromethyl)-2-pyridyl]hydrazine;[5-chloro-3-(trifluoromethyl)pyridin-2-yl]hydrazine;5-chloro-3-(trifluoromethyl)pyrid-2-yl hydrazine;SCHEMBL838690;DTXSID50369432;OYDFLZYOHRCSAV-UHFFFAOYSA-N;HMS1667G07;GS0069;MFCD00067867;CS-0216409;FT-0607166;O11400;EN300-4255982;1-[5-chloro-3-(trifluoromethyl)-2-pyridyl]hydrazine, AldrichCPR

Chemical Property of 5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine

Chemical Property:

• Vapor Pressure: 0.03mmHg at 25°C
• Melting Point: 75 °C
• Refractive Index: 1.546
• Boiling Point: 244.6 °C at 760 mmHg
• PKA: 8.10±0.70(Predicted)
• Flash Point: 101.8 °C
• PSA: 50.94000
• Density: 1.57 g/cm³
• LogP: 2.81270
• Storage Temp.: 2-8°C
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 211.0124094
• Heavy Atom Count: 13
• Complexity: 175

Purity/Quality:

99% ^*data from raw suppliers

5-Chloro-2-Hydrazinyl-3-(trifluoromethyl)pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=NC(=C1C(F)(F)F)NN)Cl

Technology Process of 5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine

There total 1 articles about 5-Chloro-2-hydrazinyl-3-(trifluoromethyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2,5-dichloro-3-(trifluoromethyl)pyridine (70158-59-7) → (5-chloro-3-(trifluoromethyl)pyridin-2-yl)hydrazine (129015-69-6)

Guidance literature:

With hydrazine hydrate; In ethanol; at 80 - 90 ℃;

DOI:10.1039/b311247k

Reference yield: 65.0%

phenyl(pyridin-2-yl)methanone (91-02-1) + (5-chloro-3-(trifluoromethyl)pyridin-2-yl)hydrazine (129015-69-6) → N-(5-Chloro-3-trifluoromethyl-pyridin-2-yl)-N'-[1-phenyl-1-pyridin-2-yl-meth-(E)-ylidene]-hydrazine

Guidance literature:

With acetic acid; In methanol; Heating;

DOI:10.1021/jm970255w

Reference yield: 63.0%

6-chloro-7-methyl-3-methylthio-1,4,2-benzodithiazin 1,1-dioxide + (5-chloro-3-(trifluoromethyl)pyridin-2-yl)hydrazine (129015-69-6) → 4-chloro-2-mercapto-5-methyl-N-(6-chloro-8-trifluoromethyl-1,2,4-triazolo<4,3-a>pyrid-3-yl)benzenesulfonamide

Guidance literature:

In toluene; Heating;

upstream raw materials:

2,5-dichloro-3-(trifluoromethyl)pyridine

Downstream raw materials:

C₁₁H₅Cl₃F₃N₅

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