(+)-5,6-o-Cyclohexylidene-l-ascorbic acid

Base Information Edit

Chemical Name:(+)-5,6-o-Cyclohexylidene-l-ascorbic acid
CAS No.:6614-52-4
Molecular Formula:C12H16O6
Molecular Weight:256.255
Hs Code.:2932999099
Mol file:6614-52-4.mol

Synonyms:(5R)-5-(1,4-dioxaspiro[4.5]decan-2-yl)-3,4-dihydroxy-5H-furan-2-one;

Suppliers and Price of (+)-5,6-o-Cyclohexylidene-l-ascorbic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(+)-5,6-O-CYCLOHEXYLIDENE-L-ASCORBIC ACID 95.00%
25G
$ 1626.30

American Custom Chemicals Corporation
(+)-5,6-O-CYCLOHEXYLIDENE-L-ASCORBIC ACID 95.00%
1G
$ 1073.89

AHH
(+)-5,6-o-Cyclohexylidene-L-ascorbic acid 98%
25g
$ 438.00

Total 8 raw suppliers

Chemical Property of (+)-5,6-o-Cyclohexylidene-l-ascorbic acid Edit

Chemical Property:

Vapor Pressure:4.89E-11mmHg at 25°C
Melting Point:180 °C (dec.)(lit.)
Refractive Index:1.589
Boiling Point:475.5 °C at 760 mmHg
Flash Point:186.8 °C
PSA：85.22000
Density:1.45 g/cm³
LogP:1.31520
Storage Temp.:2-8°C

Purity/Quality:

98% ^*data from raw suppliers

(+)-5,6-O-CYCLOHEXYLIDENE-L-ASCORBIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of (+)-5,6-o-Cyclohexylidene-l-ascorbic acid

There total 2 articles about (+)-5,6-o-Cyclohexylidene-l-ascorbic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 933-40-4
cycloxexanone dimethyl ketal

: 50-81-7,98966-42-8
ascorbic acid

: 6614-52-4
5,6-O-cyclohexylidene-L-ascorbic acid

Guidance literature:: With tin(ll) chloride; In ethyl acetate; for 0.5h; Heating;
DOI:10.1016/S0957-4166(00)82119-9

Reference yield: 88.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 26094-91-7,98966-42-8
L-arabo-ascorbic acid

: 6614-52-4,97627-84-4
5,6-O-cycloheyxlidene-(L)-ascorbic acid

Guidance literature:: With boron trifluoride diethyl etherate; orthoformic acid triethyl ester; Ambient temperature;

Reference yield: 57.0%

: 6614-52-4
5,6-O-cyclohexylidene-L-ascorbic acid

: 3958-60-9
2-nitrophenylmethyl bromide

: C₁₉H₂₁NO₈

Guidance literature:: 5,6-O-cyclohexylidene-L-ascorbic acid; With potassium carbonate; In tetrahydrofuran; dimethyl sulfoxide; for 0.5h;

2-nitrophenylmethyl bromide; In tetrahydrofuran; dimethyl sulfoxide; Inert atmosphere;