2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE

Base Information

• Chemical Name: 2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE
• CAS No.: 6758-34-5
• Molecular Formula: C9H7F3N2O
• Molecular Weight: 216.16
• Hs Code.: 2933990090
• Mol file: 6758-34-5.mol

Synonyms:2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE;5-Trifluormethyl-2-hydroxymethyl-benzimidazol;(5-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl)methanol;[5-(TrifluoroMethyl)-1H-benziMidazol-2-yl]Methanol

Chemical Property of 2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE

Chemical Property:

• Vapor Pressure: 6.42E-07mmHg at 25°C
• Boiling Point: 394.1°C at 760 mmHg
• PKA: 10.16±0.10(Predicted)
• Flash Point: 192.2°C
• PSA: 48.91000
• Density: 1.517g/cm³
• LogP: 2.07400
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

(5-(Trifluoromethyl)-1H-benzo[d]imidazol-2-yl)methanol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE

There total 2 articles about 2-(HYDROXYMETHYL)-5-TRIFLUOROMETHYL-1H-BENZOIMIDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C6H12O6 + 4-(trifluoromethyl)-1,2-phenylenediamine (368-71-8) → 5-Trifluoromethylbenzimidazole (326-55-6) + (5-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl)methanol (6758-34-5)

Guidance literature:

With di-tert-butyl peroxide; boron trifluoride diethyl etherate; In decane; acetonitrile; at 90 ℃; for 1h; Green chemistry;

DOI:10.1002/asia.202100972

Reference yield:

→ (5-(trifluoromethyl)-1H-benzo[d]imidazol-2-yl)methanol (6758-34-5)

Guidance literature:

4-Trifluormethyl-o-phenylendiamin, Glykolsaeure, konz.wss.HCl <100grad>;

upstream raw materials:

4-(trifluoromethyl)-1,2-phenylenediamine

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