3-ALLYL-2-FLUORO-4-IODO-PYRIDINE

Base Information

Chemical Name:3-ALLYL-2-FLUORO-4-IODO-PYRIDINE
CAS No.:340268-75-9
Molecular Formula:C8H7FIN
Molecular Weight:263.05
Hs Code.:2933399090
Mol file:340268-75-9.mol

Synonyms:3-ALLYL-2-FLUORO-4-IODO-PYRIDINE

Suppliers and Price of 3-ALLYL-2-FLUORO-4-IODO-PYRIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Allyl-2-fluoro-4-iodopyridine 97%
1g
$ 581.00

Chemenu
3-allyl-2-fluoro-4-iodopyridine 97%
1g
$ 549.00

American Custom Chemicals Corporation
3-ALLYL-2-FLUORO-4-IODOPYRIDINE 95.00%
1G
$ 1133.93

AK Scientific
3-Allyl-2-fluoro-4-iodopyridine
5g
$ 1686.00

AK Scientific
3-Allyl-2-fluoro-4-iodopyridine
1g
$ 525.00

AK Scientific
3-Allyl-2-fluoro-4-iodopyridine
250mg
$ 249.00

Total 9 raw suppliers

Chemical Property of 3-ALLYL-2-FLUORO-4-IODO-PYRIDINE

Chemical Property:

Boiling Point:275.6±35.0 °C(Predicted)
PKA:-1.70±0.18(Predicted)
PSA：12.89000
Density:1.715±0.06 g/cm3(Predicted)
LogP:2.55380
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

3-Allyl-2-fluoro-4-iodopyridine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-ALLYL-2-FLUORO-4-IODO-PYRIDINE

There total 3 articles about 3-ALLYL-2-FLUORO-4-IODO-PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 113975-22-7
2-fluoro-3-iodopyridine

: 106-95-6
allyl bromide

: 340268-75-9
3-allyl-2-fluoro-4-iodo-pyridine

Guidance literature:: 2-fluoro-3-iodopyridine; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

allyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1016/j.tet.2004.05.048

Reference yield:

: 372-48-5
2-fluoropyridine

: 340268-75-9
3-allyl-2-fluoro-4-iodo-pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA

1.2: 78 percent / I₂

2.1: n-BuLi; diisopropylamine / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: 87 percent / tetrahydrofuran; hexane / -78 - 20 °C

With n-butyllithium; diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1016/j.tet.2004.05.048

Reference yield:

: 340268-75-9
3-allyl-2-fluoro-4-iodo-pyridine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 ℃; for 1.5h;

In tetrahydrofuran; n-heptane; ethylbenzene; at -78 - 20 ℃; for 2.67h;