Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl--D-glucopyranoside

Base Information

• Chemical Name: Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl--D-glucopyranoside
• CAS No.: 80035-36-5
• Molecular Formula: C35H33NO7
• Molecular Weight: 579.65
• Mol file: 80035-36-5.mol

Synonyms:Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl-|A-D-glucopyranoside;

Chemical Property of Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl--D-glucopyranoside

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 732.101°C at 760 mmHg
• PKA: 12.92±0.70(Predicted)
• Flash Point: 396.56°C
• PSA: 94.53000
• Density: 1.339g/cm³
• LogP: 4.69390
• Solubility.: Acetone, Dichloromethane, Ethyl Acetate, Methanol

Purity/Quality:

99% ^*data from raw suppliers

Benzyl2-Deoxy-2-phthalimido-3,6-di-O-benzyl-β-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl--D-glucopyranoside

There total 14 articles about Benzyl 2-Deoxy-2-phthalimido-3,6-di-O-benzyl--D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C35H31NO7 → benzyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside (80035-36-5)

Guidance literature:

With trimethylamine-borane; boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1080/00397911.2013.853189

Reference yield: 83.0%

benzyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside (191482-37-8) → benzyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside (80035-36-5)

Guidance literature:

With trimethylamine-borane; boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 1h; Inert atmosphere;

Reference yield: 76.0%

benzyl 4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside → benzyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-beta-D-glucopyranoside (80035-36-5)

Guidance literature:

With methanol; sodium methylate; In dichloromethane; for 1h;

upstream raw materials:

benzyl bromide

benzyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

benzyl 2-deoxy-2-phthalimido-β-D-glucopyranoside

Downstream raw materials:

benzyl O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

C₇₇H₇₀N₂O₁₉

benzyl O-(4-O-acetyl-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Benzyl 3,6-di-O-benzyl-2-deoxy-2-amino-β-D-glucopyranoside