Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside

Base Information

Chemical Name:Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside
CAS No.:191482-37-8
Molecular Formula:C35H31NO7
Molecular Weight:577.634
Hs Code.:

Synonyms:Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside

There total 4 articles about Phenylmethyl 2-deoxy-2-(1,3-dihydro-1,3-dioxo-2H-isoindol-2-yl)-3-O-(phenylmethyl)-4,6-O-[(R)-phenylmethylene]-beta-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 100-39-0
benzyl bromide

: 149342-15-4
benzyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 191482-37-8
benzyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.166667h;
DOI:10.1021/jo962362o

Reference yield:

: 10022-13-6
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

: 191482-37-8
benzyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / conc. HCl / acetone; H₂O / 16 h / 80 °C

2: 93 percent / p-toluenesulfonic acid / acetonitrile / 15 h / Heating

3: 96 percent / NaH / dimethylformamide / 0.17 h / 0 - 20 °C

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; In water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jo962362o

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 191482-37-8
benzyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / p-toluenesulfonic acid / acetonitrile / 15 h / Heating

2: 96 percent / NaH / dimethylformamide / 0.17 h / 0 - 20 °C

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo962362o