1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

Base Information

• Chemical Name: 1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide
• CAS No.: 174899-86-6
• Molecular Formula: C6H11N2O.C2F6NO4S2
• Molecular Weight: 407.311
• European Community (EC) Number: 801-353-0
• ChEMBL ID: CHEMBL593850
• NSC Number: 747122
• Mol file: 174899-86-6.mol

Synonyms:174899-86-6;1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide;1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethanesulfonyl)imide;1-(2 inverted exclamation mark -hydroxylethyl)-3-methylimidazolium bis((trifluoromethyl)sulfonyl)imide;NSC-747122;1-(2'-hydroxylethyl)-3-methylimidazolium bis((trifluoromethyl)sulfonyl)imide;bis(trifluoromethylsulfonyl)azanide;2-(3-methylimidazol-3-ium-1-yl)ethanol;MFCD09038874;1-(2'-hydroxylethyl)-3-methylimidazoliumbis((trifluoromethyl)sulfonyl)imide;CHEMBL593850;SCHEMBL3678674;NSC747122;AKOS037648934;BS-16061;H1670;D80422;1-Ethanol-3-methylimidazolium bis(trifluoromethanesulfonyl)imide;1-(2-hydroxyethyl)-3-methylimidazolium trifluoromethanesulfonate;1-(2-hydroxyethyl)-3-methylimidazolium bis((trifluoromethyl)sulfonyl)imide;1-(2-hydroxyethyl)-3-methylimidazolium bis(trifluoromethanesulfonyl)amide;1-(2-hydroxyethyl)-3-methylimidazolium bis-(trifluoromethylsulfonyl) imide;1-(2invertedexclamationmark-hydroxylethyl)-3-methylimidazoliumbis((trifluoromethyl)sulfonyl)imide

Chemical Property of 1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

Chemical Property:

• Refractive Index: 1.43
• PSA: 114.08000
• Density: 1.57
• LogP: 2.52580
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 12
• Rotatable Bond Count: 4
• Exact Mass: 407.00443178
• Heavy Atom Count: 24
• Complexity: 461

Purity/Quality:

97% ^*data from raw suppliers

1-(2-Hydroxyethyl)-3-methylimidazolium Bis(trifluoromethanesulfonyl)imide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+]1=CN(C=C1)CCO.C(F)(F)(F)S(=O)(=O)[N-]S(=O)(=O)C(F)(F)F

Technology Process of 1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide

There total 6 articles about 1-(2-Hydroxyethyl)-3-methylimidazolium bis(trifluoromethylsulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

1-methyl-3-(2-hydroxyethyl)imidazolium bromide (97513-90-1) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → 1-(2-hydroxyethyl)-3-methylimidazolium bis((trifluoromethane)sulfonyl)amide (174899-86-6)

Guidance literature:

In water; at 20 ℃; for 2h;

Reference yield: 91.0%

bis(trifluoromethane)sulfonimide lithium (90076-65-6) + 3-(2-hydroxyethyl)-1-methyl-1H-imidazol-3-ium chloride (61755-34-8) → 1-(2-hydroxyethyl)-3-methylimidazolium bis((trifluoromethane)sulfonyl)amide (174899-86-6)

Guidance literature:

In acetonitrile; at 25 ℃; for 24h; Inert atmosphere; Green chemistry;

DOI:10.1021/op020027y

Reference yield:

C2F6NO4S2(1-)*C7H11N2O3(1+)*C9H16N2 → 1,8-diazabicyclo[5.4.0]undec-7-ene (6674-22-2,83329-50-4) + 1-(2-hydroxyethyl)-3-methylimidazolium bis((trifluoromethane)sulfonyl)amide (174899-86-6)

Guidance literature:

at 120 ℃; for 0.25h; Inert atmosphere;

DOI:10.1039/b927514b

upstream raw materials:

1-methyl-1H-imidazole

bis(trifluoromethane)sulfonimide lithium

2-bromoethanol

1-methyl-3-(2-hydroxyethyl)imidazolium bromide