3-Iodo-5-(trifluoromethyl)-2(1H)-pyridinone

Base Information

• Chemical Name: 3-Iodo-5-(trifluoromethyl)-2(1H)-pyridinone
• CAS No.: 300851-88-1
• Molecular Formula: C6H3F3INO
• Molecular Weight: 288.99
• Mol file: 300851-88-1.mol

Synonyms:3-Iodo-5-(trifluoromethyl)pyridin-2(1H)-one;3-Iodo-5-(trifluoromethyl)pyridin-2-ol;

Chemical Property of 3-Iodo-5-(trifluoromethyl)-2(1H)-pyridinone

Chemical Property:

• Boiling Point: 272 oC
• PKA: 8.10±0.10(Predicted)
• Flash Point: 118 oC
• PSA: 33.12000
• Density: 2.11
• LogP: 2.41060
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

2-Hydroxy-3-iodo-5-(trifluoromethyl)pyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T
• Hazard Codes: T
• Statements: 25
• Safety Statements: 45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Iodo-5-(trifluoromethyl)-2(1H)-pyridinone

There total 1 articles about 3-Iodo-5-(trifluoromethyl)-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-hydroxy-5-(trifluoromethyl)pyridine (33252-63-0) → 3-iodo-5-(trifluoromethyl)pyridin-2-ol (300851-88-1)

Guidance literature:

With dipotassium peroxodisulfate; cerium(III) nitrate hexahydrate; trifluoroacetic acid; sodium iodide; In 1,2-dichloro-ethane; at 130 ℃; for 24h; regioselective reaction; Molecular sieve; Inert atmosphere; Sealed tube; Schlenk technique;

DOI:10.1039/c5cc07799k

upstream raw materials:

2-hydroxy-5-(trifluoromethyl)pyridine

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