Styrene glycol dimesylate

Base Information

• Chemical Name: Styrene glycol dimesylate
• CAS No.: 32837-95-9
• Molecular Formula: C10H14O6S2
• Molecular Weight: 294.35
• Mol file: 32837-95-9.mol

Synonyms:

Chemical Property of Styrene glycol dimesylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Styrene glycol dimesylate

There total 2 articles about Styrene glycol dimesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylethane 1,2-diol (93-56-1) + methanesulfonyl chloride (124-63-0) → 1-phenylethane-1,2-diol dimethanesulphonate (32837-95-9)

Guidance literature:

With pyridine; at 0 ℃; for 4h;

DOI:10.1016/S0022-328X(00)85766-6

Reference yield:

→ 1-phenylethane-1,2-diol dimethanesulphonate (32837-95-9)

Guidance literature:

Styrol-glykol, Mesylchlorid;

Reference yield:

1-phenylethane-1,2-diol dimethanesulphonate (32837-95-9) + lithium diphenylphosphide (65567-06-8,4541-02-0) → (1-phenylethane-1,2-diyl)bis(diphenylphosphine) (69381-90-4,69381-91-5,79814-92-9,121902-83-8)

Guidance literature:

In tetrahydrofuran; at -78 - 20 ℃; Schlenk technique;

DOI:10.1021/cs400651h

upstream raw materials:

phenylethane 1,2-diol

methanesulfonyl chloride

Downstream raw materials:

(1-phenylethane-1,2-diyl)bis(diphenylphosphine)