1-BENZYL-3-N-BOC-AMINOPIPERIDINE

Base Information

• Chemical Name: 1-BENZYL-3-N-BOC-AMINOPIPERIDINE
• CAS No.: 478828-62-5
• Molecular Formula: C17H26N2O2
• Molecular Weight: 290.406
• Hs Code.: 29333990
• Mol file: 478828-62-5.mol

Synonyms:tert-Butyl (1-benzylpiperidin-3-yl)carbamate;(1-Benzyl-piperidin-3-yl)-carbamic acid tert-butyl ester;(tert-Butoxy)-N-[1-benzyl(3-piperidyl)]carboxamide;

Chemical Property of 1-BENZYL-3-N-BOC-AMINOPIPERIDINE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 118 - 120 °C
• Refractive Index: 1.542
• Boiling Point: 400.862 °C at 760 mmHg
• Flash Point: 196.235 °C
• PSA: 41.57000
• Density: 1.076 g/cm³
• LogP: 3.50450

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl(1-benzylpiperidin-3-yl)carbamate 97% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-BENZYL-3-N-BOC-AMINOPIPERIDINE

There total 15 articles about 1-BENZYL-3-N-BOC-AMINOPIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-((tert-butoxycarbonyl)amino)penta-1,5-diyl dimesylate + benzylamine (100-46-9) → (1-benzylpiperidin-3-yl)carbamic acid tert-butyl ester (478828-62-5,216854-24-9)

Guidance literature:

In dichloromethane; at 45 ℃;

Reference yield: 95.0%

di-tert-butyl dicarbonate (24424-99-5) + 1-phenylmethyl-3-aminopiperidine (60407-35-4) → (1-benzylpiperidin-3-yl)carbamic acid tert-butyl ester (478828-62-5,216854-24-9)

Guidance literature:

With lanthanum(III) nitrate; at 20 ℃; for 0.05h;

DOI:10.1016/j.tetlet.2006.09.081

Reference yield: 77.0%

N-benzyl-3-((tert-butoxycarbonyl)amino)pyridinium bromide (1415146-39-2) → (1-benzylpiperidin-3-yl)carbamic acid tert-butyl ester (478828-62-5,216854-24-9)

Guidance literature:

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; triethylammonium formate; potassium iodide; In dichloromethane; at 40 ℃; for 24h; Sealed tube;

DOI:10.1002/adsc.201201034

upstream raw materials:

di-tert-butyl dicarbonate

1-phenylmethyl-3-aminopiperidine

1-benzylpiperidine-3-carboxylic acid

tert-butyl alcohol

Downstream raw materials:

1-phenylmethyl-3-aminopiperidine

t-butyl piperidin-3-ylcarbamate

3-amino-1-benzylpiperidine dihydrochloride

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